5,12-bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Base Information

• Chemical Name: 5,12-bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone
• CAS No.: 876301-65-4
• Molecular Formula: C₆₈H₈₂N₂O₆
• Molecular Weight: 1023.41
• Mol file: 876301-65-4.mol

Synonyms:5,12-bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Chemical Property of 5,12-bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,12-bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

There total 2 articles about 5,12-bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

2-Ethylhexylamine (104-75-6) + 1,7-(3’,5‘-di-t-butylphenoxy)perylene-3,4:9,10-tetracarboxydianhydride (404871-21-2) → 5,12-bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone (876301-65-4)

Guidance literature:

With pyridine; for 12h; Heating;

DOI:10.1021/ja057031k

Reference yield:

2-Ethylhexylamine (104-75-6) + 1,7-(3’,5‘-di-t-butylphenoxy)perylene-3,4:9,10-tetracarboxydianhydride (404871-21-2) → N-(2-ethylhexyl)-1,7-(3’,5’-di-t-butylphenoxy)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide (457892-77-2) + 5,12-bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone (876301-65-4)

Guidance literature:

With pyridine; for 2h; Heating;

DOI:10.1021/ja0398215

Reference yield:

5,12-bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone (876301-65-4) → 5,12-Bis-(3,5-di-tert-butyl-phenoxy)-2,9-bis-(2-ethyl-hexyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Guidance literature:

With triethylamine; In dichloromethane; Photolysis;

DOI:10.1021/ja057031k

upstream raw materials:

2-Ethylhexylamine

1,7-(3’,5‘-di-t-butylphenoxy)perylene-3,4:9,10-tetracarboxydianhydride