(2S)-N-(2-benzyloxycarbonylamino-4-methylpentyloxycarbonyloxy)sucinimide

Base Information

Chemical Name:(2S)-N-(2-benzyloxycarbonylamino-4-methylpentyloxycarbonyloxy)sucinimide
CAS No.:73352-53-1
Molecular Formula:C₁₉H₂₄N₂O₇
Molecular Weight:392.409
Hs Code.:

Synonyms:(2S)-N-(2-benzyloxycarbonylamino-4-methylpentyloxycarbonyloxy)sucinimide

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Chemical Property of (2S)-N-(2-benzyloxycarbonylamino-4-methylpentyloxycarbonyloxy)sucinimide

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Technology Process of (2S)-N-(2-benzyloxycarbonylamino-4-methylpentyloxycarbonyloxy)sucinimide

There total 5 articles about (2S)-N-(2-benzyloxycarbonylamino-4-methylpentyloxycarbonyloxy)sucinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: C₁₅H₂₀ClNO₄

: 73352-53-1
(2S)-N-(2-benzyloxycarbonylamino-4-methylpentyloxycarbonyloxy)sucinimide

Guidance literature:: With pyridine; In ethyl acetate; at 25 ℃; for 1.5h;
DOI:10.1039/P19810002186

Reference yield:

: 6216-61-1
(S)-(-)-N-(benzyloxycarbonyl)leucinol

: 73352-53-1
(2S)-N-(2-benzyloxycarbonylamino-4-methylpentyloxycarbonyloxy)sucinimide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 3 h

2: 84 percent / pyridine / ethyl acetate / 1.5 h / 25 °C

With pyridine; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1039/P19810002186

Reference yield:

: 7533-40-6,14438-11-0
(S)-2-amino-4-methylpentan-1-ol

: 73352-53-1
(2S)-N-(2-benzyloxycarbonylamino-4-methylpentyloxycarbonyloxy)sucinimide

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / sodium carbonate / acetone; H₂O / 3 h / 0 °C

2: triethylamine / CH₂Cl₂ / 3 h

3: 84 percent / pyridine / ethyl acetate / 1.5 h / 25 °C

With pyridine; sodium carbonate; triethylamine; In dichloromethane; water; ethyl acetate; acetone;
DOI:10.1039/P19810002186