(C₅H₄N)2C₅H₂NC₆H₄NHCOCH₂CH₂C₄NH(CH₃)(COOH)CONHC(NH₂)2⁽¹⁺⁾*Cl^(1-)=[C₃₂H₂₉N₈O₄]Cl

Base Information

• Chemical Name: (C₅H₄N)2C₅H₂NC₆H₄NHCOCH₂CH₂C₄NH(CH₃)(COOH)CONHC(NH₂)2⁽¹⁺⁾*Cl^(1-)=[C₃₂H₂₉N₈O₄]Cl
• CAS No.: 1309474-97-2
• Molecular Formula: C₃₂H₂₈N₈O₄*ClH
• Molecular Weight: 625.086

Synonyms:(C₅H₄N)2C₅H₂NC₆H₄NHCOCH₂CH₂C₄NH(CH₃)(COOH)CONHC(NH₂)2⁽¹⁺⁾*Cl^(1-)=[C₃₂H₂₉N₈O₄]Cl

Chemical Property of (C₅H₄N)2C₅H₂NC₆H₄NHCOCH₂CH₂C₄NH(CH₃)(COOH)CONHC(NH₂)2⁽¹⁺⁾*Cl^(1-)=[C₃₂H₂₉N₈O₄]Cl

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Technology Process of (C₅H₄N)2C₅H₂NC₆H₄NHCOCH₂CH₂C₄NH(CH₃)(COOH)CONHC(NH₂)2⁽¹⁺⁾*Cl^(1-)=[C₃₂H₂₉N₈O₄]Cl

There total 6 articles about (C₅H₄N)2C₅H₂NC₆H₄NHCOCH₂CH₂C₄NH(CH₃)(COOH)CONHC(NH₂)2⁽¹⁺⁾*Cl^(1-)=[C₃₂H₂₉N₈O₄]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(C5H4N)2(C5H2N)C6H4NHC(O)CH2CH2(C4NH)(CH3)(C(O)OC(CH3)3)C(O)NHC(NH)NHC(O)OC(CH3)3 (1135134-66-5) → (C5H4N)2C5H2NC6H4NHCOCH2CH2C4NH(CH3)(COOH)CONHC(NH2)2(1+)*Cl(1-)=[C32H29N8O4]Cl (1309474-97-2)

Guidance literature:

(C₅H₄N)2(C₅H₂N)C₆H₄NHC(O)CH₂CH₂(C₄NH)(CH₃)(C(O)OC(CH₃)3)C(O)NHC(NH)NHC(O)OC(CH₃)3; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 336h;

With hydrogenchloride; In water;

DOI:10.1021/ja200941a

Reference yield:

3-(5-(tert-butoxycarbonyl)-2-(N-(tert-butoxycarbonyl)carbamimidoylcarbamoyl)-4-methyl-1H-pyrrol-3-yl)propanoic acid (1245792-37-3) → (C5H4N)2C5H2NC6H4NHCOCH2CH2C4NH(CH3)(COOH)CONHC(NH2)2(1+)*Cl(1-)=[C32H29N8O4]Cl (1309474-97-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 4-methyl-morpholine; HATU / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

1.2: 62 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 336 h / 20 °C

With 4-methyl-morpholine; HATU; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja200941a

Reference yield:

4′-(4-amino-phenyl)-2,2′:6′,2′′-terpyridine (178265-65-1) → (C5H4N)2C5H2NC6H4NHCOCH2CH2C4NH(CH3)(COOH)CONHC(NH2)2(1+)*Cl(1-)=[C32H29N8O4]Cl (1309474-97-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 4-methyl-morpholine; HATU / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

1.2: 62 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 336 h / 20 °C

With 4-methyl-morpholine; HATU; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja200941a

upstream raw materials:

(C₅H₄N)2(C₅H₂N)C₆H₄NHC(O)CH₂CH₂(C₄NH)(CH₃)(C(O)OC(CH₃)3)C(O)NHC(NH)NHC(O)OC(CH₃)3

3-(5-(tert-butoxycarbonyl)-2-(N-(tert-butoxycarbonyl)carbamimidoylcarbamoyl)-4-methyl-1H-pyrrol-3-yl)propanoic acid

tert-butyl 5-(N-(tert-butoxycarbonyl)carbamimidoylcarbamoyl)-4-(3-methoxy-3-oxopropyl)-3-methyl-1H-pyrrole-2-carboxylate

benzyl 5-acetoxymethyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrole-2-carboxylate

Downstream raw materials:

(C₅H₄N)2(C₅H₂N)C₆H₄NHC(O)CH₂CH₂(C₄NH)(CH₃)(C(O)OH)C(O)NHC(NH)NH₂

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