Technology Process of C12H14BrN3O
There total 6 articles about C12H14BrN3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
for 1.5h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: manganese(IV) oxide / chloroform
2.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C
2.2: 18 h / 0 - 20 °C
3.1: sodium hydroxide / tetrahydrofuran; methanol / 8 h / 20 °C
4.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C
4.2: 16 h
5.1: trifluoroacetic acid / 1.5 h
With
manganese(IV) oxide; sodium hydride; 1,1'-carbonyldiimidazole; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.25 h / Cooling with ice
1.2: Cooling with ice
2.1: manganese(IV) oxide / chloroform
3.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C
3.2: 18 h / 0 - 20 °C
4.1: sodium hydroxide / tetrahydrofuran; methanol / 8 h / 20 °C
5.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C
5.2: 16 h
6.1: trifluoroacetic acid / 1.5 h
With
manganese(IV) oxide; chloroformic acid ethyl ester; sodium hydride; triethylamine; 1,1'-carbonyldiimidazole; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide;
