benzyl (cis-6-(4-hexylbenzoyl)-cis-4-(phenylsulfonyl)-2-cyclohexen-1-yl)carbamate

Base Information

Chemical Name:benzyl (cis-6-(4-hexylbenzoyl)-cis-4-(phenylsulfonyl)-2-cyclohexen-1-yl)carbamate
CAS No.:131906-68-8
Molecular Formula:C₃₃H₃₇NO₅S
Molecular Weight:559.726
Hs Code.:

Synonyms:benzyl (cis-6-(4-hexylbenzoyl)-cis-4-(phenylsulfonyl)-2-cyclohexen-1-yl)carbamate

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Chemical Property of benzyl (cis-6-(4-hexylbenzoyl)-cis-4-(phenylsulfonyl)-2-cyclohexen-1-yl)carbamate

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Technology Process of benzyl (cis-6-(4-hexylbenzoyl)-cis-4-(phenylsulfonyl)-2-cyclohexen-1-yl)carbamate

There total 3 articles about benzyl (cis-6-(4-hexylbenzoyl)-cis-4-(phenylsulfonyl)-2-cyclohexen-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 131906-57-5
1-(4-hexylphenyl)-2-propen-1-one

: 86802-64-4
((1E,3E)-4-Benzenesulfonyl-buta-1,3-dienyl)-carbamic acid benzyl ester

: 131906-68-8
benzyl (cis-6-(4-hexylbenzoyl)-cis-4-(phenylsulfonyl)-2-cyclohexen-1-yl)carbamate

Guidance literature:: With 4-tert-Butylcatechol; In 1,4-dioxane; water; at 50 ℃; for 25h;
DOI:10.1021/jo00007a041

Reference yield:

: 79219-16-2
1-(4-hexyl-phenyl)-propan-1-one

: 131906-68-8
benzyl (cis-6-(4-hexylbenzoyl)-cis-4-(phenylsulfonyl)-2-cyclohexen-1-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: conc. hydrochloric acid / ethyl acetate / 24 h / 25 °C

2: NaIO₄, NaHCO₃ / methanol; H₂O / 1 h / 25 °C

3: 68 percent / 4-tert-butylcatechol / dioxane; H₂O / 25 h / 50 °C

With hydrogenchloride; sodium periodate; 4-tert-Butylcatechol; sodium hydrogencarbonate; In 1,4-dioxane; methanol; water; ethyl acetate;
DOI:10.1021/jo00007a041

Reference yield:

: 131906-71-3
1-(4-Hexyl-phenyl)-2-phenylselanyl-propan-1-one

: 131906-68-8
benzyl (cis-6-(4-hexylbenzoyl)-cis-4-(phenylsulfonyl)-2-cyclohexen-1-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: NaIO₄, NaHCO₃ / methanol; H₂O / 1 h / 25 °C

2: 68 percent / 4-tert-butylcatechol / dioxane; H₂O / 25 h / 50 °C

With sodium periodate; 4-tert-Butylcatechol; sodium hydrogencarbonate; In 1,4-dioxane; methanol; water;
DOI:10.1021/jo00007a041