1-benzylcyclobutanecarbonyl azide

Base Information

Chemical Name:1-benzylcyclobutanecarbonyl azide
CAS No.:1255306-38-7
Molecular Formula:C₁₂H₁₃N₃O
Molecular Weight:215.255
Hs Code.:

Synonyms:1-benzylcyclobutanecarbonyl azide

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Chemical Property of 1-benzylcyclobutanecarbonyl azide

Chemical Property:

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Technology Process of 1-benzylcyclobutanecarbonyl azide

There total 3 articles about 1-benzylcyclobutanecarbonyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 114672-02-5
1-benzylcyclobutane-1-carboxylic acid

: 1255306-38-7
1-benzylcyclobutanecarbonyl azide

Guidance literature:: 1-benzylcyclobutane-1-carboxylic acid; With chloroformic acid ethyl ester; triethylamine; In water; acetone; at 0 ℃;

With sodium azide; In water; at 0 ℃; for 1h;

Reference yield:

: 100-39-0
benzyl bromide

: 1255306-38-7
1-benzylcyclobutanecarbonyl azide

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C

2.1: sodium hydroxide; ethanol / Reflux

2.2: pH 3 - 4

3.1: triethylamine; methyl chloroformate / water; acetone / 1 h / 0 °C

With ethanol; triethylamine; methyl chloroformate; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; water; acetone;

Reference yield:

: 114672-01-4
ethyl 1-benzylcyclobutane-1-carboxylate

: 1255306-38-7
1-benzylcyclobutanecarbonyl azide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; ethanol / Reflux

1.2: pH 3 - 4

2.1: triethylamine; methyl chloroformate / water; acetone / 1 h / 0 °C

With ethanol; triethylamine; methyl chloroformate; sodium hydroxide; In water; acetone;