Benzoic acid (Z)-(1R,2R)-2-amino-1-methyl-hexa-3,5-dienyl ester; hydrochloride

Base Information

Chemical Name:Benzoic acid (Z)-(1R,2R)-2-amino-1-methyl-hexa-3,5-dienyl ester; hydrochloride
CAS No.:88549-80-8
Molecular Formula:C₁₄H₁₇NO₂*ClH
Molecular Weight:267.755
Hs Code.:

Synonyms:Benzoic acid (Z)-(1R,2R)-2-amino-1-methyl-hexa-3,5-dienyl ester; hydrochloride

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Chemical Property of Benzoic acid (Z)-(1R,2R)-2-amino-1-methyl-hexa-3,5-dienyl ester; hydrochloride

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Technology Process of Benzoic acid (Z)-(1R,2R)-2-amino-1-methyl-hexa-3,5-dienyl ester; hydrochloride

There total 2 articles about Benzoic acid (Z)-(1R,2R)-2-amino-1-methyl-hexa-3,5-dienyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 88549-79-5
(4R,5R)-4-((E)-Buta-1,3-dienyl)-5-methyl-2-phenyl-4,5-dihydro-oxazole

: 88549-80-8
Benzoic acid (Z)-(1R,2R)-2-amino-1-methyl-hexa-3,5-dienyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; at 40 ℃;
DOI:10.1021/ja00316a062

Reference yield:

: 88549-78-4
Toluene-4-sulfonate((4S,5R)-5-methyl-2-phenyl-4,5-dihydro-oxazol-4-ylmethyl)-triphenyl-phosphonium;

: 88549-80-8
Benzoic acid (Z)-(1R,2R)-2-amino-1-methyl-hexa-3,5-dienyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 1.) n-BuLi / 2.) THF, -78 degC

2: 95 percent / 1 N HCl / 40 °C

With hydrogenchloride; n-butyllithium;
DOI:10.1021/ja00316a062

Reference yield:

: 88549-80-8
Benzoic acid (Z)-(1R,2R)-2-amino-1-methyl-hexa-3,5-dienyl ester; hydrochloride

: 88549-82-0
(1R,3aR,4R,7aR)-1-((R)-1-Benzyloxy-ethyl)-3-oxo-2,3,3a,4,5,7a-hexahydro-1H-isoindole-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylimidazole / tetrahydrofuran / -70 degC to r.t.

2: 97 percent / benzene / 2 h / 180 °C

With 1-methyl-1H-imidazole; In tetrahydrofuran; benzene;
DOI:10.1021/ja00316a062