(S)-1-(3-((2-(tert-butoxycarbonylamino)propionylamino)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid hydrazide

Base Information

Chemical Name:(S)-1-(3-((2-(tert-butoxycarbonylamino)propionylamino)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid hydrazide
CAS No.:895524-51-3
Molecular Formula:C₂₀H₂₅F₃N₆O₄
Molecular Weight:470.452
Hs Code.:

Synonyms:(S)-1-(3-((2-(tert-butoxycarbonylamino)propionylamino)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid hydrazide

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Chemical Property of (S)-1-(3-((2-(tert-butoxycarbonylamino)propionylamino)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid hydrazide

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Technology Process of (S)-1-(3-((2-(tert-butoxycarbonylamino)propionylamino)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid hydrazide

There total 2 articles about (S)-1-(3-((2-(tert-butoxycarbonylamino)propionylamino)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1059538-97-4
(S)-methyl 1-(3-((2-(tert-butoxycarbonylamino)propanamido)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylate

: 895524-51-3
(S)-1-(3-((2-(tert-butoxycarbonylamino)propionylamino)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid hydrazide

Guidance literature:: With hydrazine hydrate; for 0.5h; Heating;
DOI:10.1016/j.bmcl.2009.04.075

Reference yield:

: 895524-50-2
C₂₂H₂₇F₃N₄O₅

: 895524-51-3
(S)-1-(3-((2-(tert-butoxycarbonylamino)propionylamino)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid hydrazide

Guidance literature:: With hydrazine; In ethanol; at 60 ℃; for 6h;

Reference yield:

: 895524-51-3
(S)-1-(3-((2-(tert-butoxycarbonylamino)propionylamino)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid hydrazide

: 103-72-0
phenyl isothiocyanate

: 895524-52-4
tert-butyl (S)-1-(3-(5-(5-(phenylamino)-1,3,4-oxadiazol-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl)benzylamino)-1-oxopropan-2-ylcarbamate

Guidance literature:: (S)-1-(3-((2-(tert-butoxycarbonylamino)propionylamino)methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid hydrazide; phenyl isothiocyanate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

In N,N-dimethyl-formamide; at 80 ℃; for 24h;

With polystyrene-bound 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;