C₂₂H₂₅N

Base Information

• Chemical Name: C₂₂H₂₅N
• CAS No.: 1419174-74-5
• Molecular Formula: C₂₂H₂₅N
• Molecular Weight: 303.447

Synonyms:C₂₂H₂₅N

Chemical Property of C₂₂H₂₅N

Chemical Property:

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Technology Process of C₂₂H₂₅N

There total 3 articles about C₂₂H₂₅N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-bromophenyl)cyclohexane-1-carbonitrile (626603-27-8) + (4-isopropylphenyl)boronic acid (16152-51-5) → C22H25N (1419174-74-5)

Guidance literature:

With potassium carbonate; palladium dichloride; In ethanol; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/ol303569b

Reference yield:

4-Bromophenylacetonitrile (16532-79-9) → C22H25N (1419174-74-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / dimethyl sulfoxide / 1 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: palladium dichloride; potassium carbonate / ethanol / 0.5 h / 20 °C / Inert atmosphere

With sodium hydride; potassium carbonate; palladium dichloride; In ethanol; dimethyl sulfoxide; 2.1: |Suzuki Coupling;

DOI:10.1021/ol303569b

Reference yield:

1,5-dibromo-pentane (111-24-0) → C22H25N (1419174-74-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / dimethyl sulfoxide / 1 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: palladium dichloride; potassium carbonate / ethanol / 0.5 h / 20 °C / Inert atmosphere

With sodium hydride; potassium carbonate; palladium dichloride; In ethanol; dimethyl sulfoxide; 2.1: |Suzuki Coupling;

DOI:10.1021/ol303569b

upstream raw materials:

1-(4-bromophenyl)cyclohexane-1-carbonitrile

(4-isopropylphenyl)boronic acid

4-Bromophenylacetonitrile

1,5-dibromo-pentane

Downstream raw materials:

1-(4'-isopropyl-[1,1'-biphenyl]-4-yl)cyclohexanecarboxylic acid

6-(4-isopropylphenyl)-2H-spiro[benzofuran-3,1'-cyclohexan]-2-one

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