(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[naphthalen-2-ylcarbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate

Base Information

Chemical Name:(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[naphthalen-2-ylcarbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate
CAS No.:1559057-65-6
Molecular Formula:C₄₇H₄₆F₂O₇
Molecular Weight:760.875
Hs Code.:

(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[naphthalen-2-ylcarbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate

Synonyms:(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[naphthalen-2-ylcarbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate

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Chemical Property of (1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[naphthalen-2-ylcarbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate

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Technology Process of (1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[naphthalen-2-ylcarbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate

There total 4 articles about (1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[naphthalen-2-ylcarbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1559057-51-0
(1S,2R,3R,4R)-4-[(naphthalen-2-yl)carbonyloxy]-3-[(1E)-3-oxo-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate

: 1559057-65-6
(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[naphthalen-2-ylcarbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate

Guidance literature:: With DeoxoFluor; In toluene; at 25 ℃; for 24h;

Reference yield:

: 1559057-77-0,130209-78-8
C₂₅H₃₆O₆

: 1559057-65-6
(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[naphthalen-2-ylcarbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; 1,4-dioxane / 11 h / 25 - 40 °C

2: pyridine / dichloromethane / 7 h / 5 - 25 °C

3: DeoxoFluor / toluene / 24 h / 25 °C

With pyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; dichloromethane; toluene;

Reference yield:

: 1559057-74-7
(Z)-isopropyl 7-((1R,5S,6R,7R)-7-((E)-3-hydroxy-4-phenoxybut-1-en-1-yl)-3-phenyl-2,4-dioxa-3-borabicyclo[3.2.1]octan-6-yl)hept-5-enoate

: 1559057-65-6
(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[naphthalen-2-ylcarbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl naphthalene-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: PCC on alumina / dichloromethane / 3 h / 25 °C

2: pyridine / dichloromethane / 7 h / 5 - 25 °C

3: DeoxoFluor / toluene / 24 h / 25 °C

With pyridine; PCC on alumina; In dichloromethane; toluene;