2-(3-(2-hydroxyethyl)ureido)-N-(3-methylbenzyl)-1H-benzo[d]imidazole-5-sulfonamide

Base Information

Chemical Name:2-(3-(2-hydroxyethyl)ureido)-N-(3-methylbenzyl)-1H-benzo[d]imidazole-5-sulfonamide
CAS No.:1422695-62-2
Molecular Formula:C₁₈H₂₁N₅O₄S
Molecular Weight:403.462
Hs Code.:

Synonyms:2-(3-(2-hydroxyethyl)ureido)-N-(3-methylbenzyl)-1H-benzo[d]imidazole-5-sulfonamide

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Chemical Property of 2-(3-(2-hydroxyethyl)ureido)-N-(3-methylbenzyl)-1H-benzo[d]imidazole-5-sulfonamide

Chemical Property:

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Technology Process of 2-(3-(2-hydroxyethyl)ureido)-N-(3-methylbenzyl)-1H-benzo[d]imidazole-5-sulfonamide

There total 4 articles about 2-(3-(2-hydroxyethyl)ureido)-N-(3-methylbenzyl)-1H-benzo[d]imidazole-5-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1375830-52-6
C₁₇H₁₈N₄O₄S

: 141-43-5
ethanolamine

: 1422695-62-2
2-(3-(2-hydroxyethyl)ureido)-N-(3-methylbenzyl)-1H-benzo[d]imidazole-5-sulfonamide

Guidance literature:: With pyridine; at 90 - 100 ℃; for 3h;
DOI:10.1016/j.ejmech.2012.11.005

Reference yield:

: 934-32-7
1H-benzimidazol-2-amine

: 1422695-62-2
2-(3-(2-hydroxyethyl)ureido)-N-(3-methylbenzyl)-1H-benzo[d]imidazole-5-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutylammomium bromide; calcium chloride / 6 h / 90 - 100 °C

2: chlorosulfonic acid / ethyl acetate / 0 °C

3: triethylamine / tetrahydrofuran / 20 °C

4: pyridine / 3 h / 90 - 100 °C

With pyridine; chlorosulfonic acid; tetrabutylammomium bromide; triethylamine; calcium chloride; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.ejmech.2012.11.005

Reference yield:

: 79213-74-4
methyl [6-(chlorosulfonyl)-1H-benzo[d]imidazol-2-yl]-carbamate

: 1422695-62-2
2-(3-(2-hydroxyethyl)ureido)-N-(3-methylbenzyl)-1H-benzo[d]imidazole-5-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 20 °C

2: pyridine / 3 h / 90 - 100 °C

With pyridine; triethylamine; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2012.11.005