5-(5-methyl-1-phenyl-1H-[1,2,3]triazol-4-yl)-4-phenyl-2,4-dihydro-[1,2,4]triazole-3-thione

Base Information

• Chemical Name: 5-(5-methyl-1-phenyl-1H-[1,2,3]triazol-4-yl)-4-phenyl-2,4-dihydro-[1,2,4]triazole-3-thione
• CAS No.: 342006-10-4
• Molecular Formula: C₁₇H₁₄N₆S
• Molecular Weight: 334.404

Synonyms:5-(5-methyl-1-phenyl-1H-[1,2,3]triazol-4-yl)-4-phenyl-2,4-dihydro-[1,2,4]triazole-3-thione

Chemical Property of 5-(5-methyl-1-phenyl-1H-[1,2,3]triazol-4-yl)-4-phenyl-2,4-dihydro-[1,2,4]triazole-3-thione

Chemical Property:

Purity/Quality:

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Technology Process of 5-(5-methyl-1-phenyl-1H-[1,2,3]triazol-4-yl)-4-phenyl-2,4-dihydro-[1,2,4]triazole-3-thione

There total 3 articles about 5-(5-methyl-1-phenyl-1H-[1,2,3]triazol-4-yl)-4-phenyl-2,4-dihydro-[1,2,4]triazole-3-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

2-(5-methyl-1- phenyl-1H- 1,2,3- triazole-4-carbonyl)-N-phenylhydrazinecar-bothioamide (342005-98-5) → 5-(5-methyl-1-phenyl-1H-[1,2,3]triazol-4-yl)-4-phenyl-2,4-dihydro-[1,2,4]triazole-3-thione (342006-10-4)

Guidance literature:

With sodium hydroxide; for 6h; Heating;

DOI:10.1002/jccs.200100022

Reference yield:

phenyl isothiocyanate (103-72-0) → 5-(5-methyl-1-phenyl-1H-[1,2,3]triazol-4-yl)-4-phenyl-2,4-dihydro-[1,2,4]triazole-3-thione (342006-10-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / ethanol / 5 h / 20 °C

2: 81 percent / 8 percent aq. NaOH / 6 h / Heating

With sodium hydroxide; In ethanol;

DOI:10.1002/jccs.200100022

Reference yield:

1-phenyl-5-methyl-1,2,3-triazol-4-formyl hydrazide (91129-91-8) → 5-(5-methyl-1-phenyl-1H-[1,2,3]triazol-4-yl)-4-phenyl-2,4-dihydro-[1,2,4]triazole-3-thione (342006-10-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / ethanol / 5 h / 20 °C

2: 81 percent / 8 percent aq. NaOH / 6 h / Heating

With sodium hydroxide; In ethanol;

DOI:10.1002/jccs.200100022

upstream raw materials:

2-(5-methyl-1- phenyl-1H- 1,2,3- triazole-4-carbonyl)-N-phenylhydrazinecar-bothioamide

phenyl isothiocyanate

1-phenyl-5-methyl-1,2,3-triazol-4-formyl hydrazide

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