(E,E)-2-[2-(tert-butyldimethylsilyloxy)ethyl]-5-(4-methoxy-phenyl)penta-2,4-dien-1-al

Base Information

Chemical Name:(E,E)-2-[2-(tert-butyldimethylsilyloxy)ethyl]-5-(4-methoxy-phenyl)penta-2,4-dien-1-al
CAS No.:1227391-18-5
Molecular Formula:C₂₀H₃₀O₃Si
Molecular Weight:346.542
Hs Code.:

Synonyms:(E,E)-2-[2-(tert-butyldimethylsilyloxy)ethyl]-5-(4-methoxy-phenyl)penta-2,4-dien-1-al

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E,E)-2-[2-(tert-butyldimethylsilyloxy)ethyl]-5-(4-methoxy-phenyl)penta-2,4-dien-1-al

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Technology Process of (E,E)-2-[2-(tert-butyldimethylsilyloxy)ethyl]-5-(4-methoxy-phenyl)penta-2,4-dien-1-al

There total 1 articles about (E,E)-2-[2-(tert-butyldimethylsilyloxy)ethyl]-5-(4-methoxy-phenyl)penta-2,4-dien-1-al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₉NO₂Si

: 1227391-18-5
(E,E)-2-[2-(tert-butyldimethylsilyloxy)ethyl]-5-(4-methoxy-phenyl)penta-2,4-dien-1-al

Guidance literature:: With water; oxalic acid; In tert-butyl methyl ether; for 2.5h;
DOI:10.1007/s11172-010-0008-4

Reference yield: 90.0%

: 1227391-18-5
(E,E)-2-[2-(tert-butyldimethylsilyloxy)ethyl]-5-(4-methoxy-phenyl)penta-2,4-dien-1-al

: 1306615-79-1
(2E,4E)-2-(2-tert-butyldimethylsilyloxyethyl)-5-(4-methoxyphenyl)penta-2,4-dien-1-ol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 2h;
DOI:10.1007/s11172-010-0359-x

Reference yield:

: 1227391-18-5
(E,E)-2-[2-(tert-butyldimethylsilyloxy)ethyl]-5-(4-methoxy-phenyl)penta-2,4-dien-1-al

: 1257303-45-9
(3Z,5E)-6-(4-methoxyphenyl)-3-methylhexa-3,5-dien-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / ethanol / 2 h / 20 °C

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; p-toluenesulfonyl chloride / diethyl ether; hexane / 2.5 h / 0 °C / Inert atmosphere

2.2: -15 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.83 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; n-butyllithium; tetrabutyl ammonium fluoride; p-toluenesulfonyl chloride; In tetrahydrofuran; diethyl ether; ethanol; hexane;
DOI:10.1007/s11172-010-0359-x