(2Z,4E)-2,3,4-Triethyl-hepta-2,4-dienoic acid (2,6-dichloro-phenyl)-amide

Base Information

• Chemical Name: (2Z,4E)-2,3,4-Triethyl-hepta-2,4-dienoic acid (2,6-dichloro-phenyl)-amide
• CAS No.: 858947-65-6
• Molecular Formula: C₁₉H₂₅Cl₂NO
• Molecular Weight: 354.32
• Mol file: 858947-65-6.mol

Synonyms:(2Z,4E)-2,3,4-Triethyl-hepta-2,4-dienoic acid (2,6-dichloro-phenyl)-amide

Chemical Property of (2Z,4E)-2,3,4-Triethyl-hepta-2,4-dienoic acid (2,6-dichloro-phenyl)-amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2Z,4E)-2,3,4-Triethyl-hepta-2,4-dienoic acid (2,6-dichloro-phenyl)-amide

There total 1 articles about (2Z,4E)-2,3,4-Triethyl-hepta-2,4-dienoic acid (2,6-dichloro-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2,6-dichlorophenylisocyanate (39920-37-1) + 4,5-diethyl-3-iodoocta-(3Z,5E)-3,5-diene (193211-59-5) → (2Z,4E)-2,3,4-Triethyl-hepta-2,4-dienoic acid (2,6-dichloro-phenyl)-amide (858947-65-6)

Guidance literature:

4,5-diethyl-3-iodoocta-(3Z,5E)-3,5-diene; With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; for 1h;

2,6-dichlorophenylisocyanate; In diethyl ether; pentane; at 20 ℃; for 2h;

DOI:10.1021/jo050433q

Reference yield: 95.0%

(2Z,4E)-2,3,4-Triethyl-hepta-2,4-dienoic acid (2,6-dichloro-phenyl)-amide (858947-65-6) → [5-(1-bromo-propyl)-3,4,5-triethyl-5H-furan-2-ylidene]-(2,6-dichloro-phenyl)-amine

Guidance literature:

With N-Bromosuccinimide; In tetrahydrofuran; water; at 20 ℃; for 3h;

DOI:10.1021/jo050433q

Reference yield: 91.0%

(2Z,4E)-2,3,4-Triethyl-hepta-2,4-dienoic acid (2,6-dichloro-phenyl)-amide (858947-65-6) → (2,6-dichloro-phenyl)-(3,4,5-triethyl-5-propyl-5H-furan-2-ylidene)-amine

Guidance literature:

With hydrogenchloride; In diethyl ether; at 20 ℃; for 18h;

DOI:10.1021/jo050433q

upstream raw materials:

2,6-dichlorophenylisocyanate

4,5-diethyl-3-iodoocta-(3Z,5E)-3,5-diene