tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-nitrophenyl)hydroxyethyl)amino)butylcarbamate

Base Information

• Chemical Name: tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-nitrophenyl)hydroxyethyl)amino)butylcarbamate
• CAS No.: 1068147-86-3
• Molecular Formula: C₃₁H₃₉N₃O₆
• Molecular Weight: 549.667

Synonyms:tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-nitrophenyl)hydroxyethyl)amino)butylcarbamate

Chemical Property of tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-nitrophenyl)hydroxyethyl)amino)butylcarbamate

Chemical Property:

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Technology Process of tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-nitrophenyl)hydroxyethyl)amino)butylcarbamate

There total 1 articles about tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-nitrophenyl)hydroxyethyl)amino)butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

N(1)-benzyl-N(4)-(tert-butyloxycarbonyl)-1,4-diaminobutane (90914-09-3) + 2-(3-benzyloxy-4-nitrophenyl)oxirane (51582-41-3) → tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-nitrophenyl)hydroxyethyl)amino)butylcarbamate (1068147-86-3)

Guidance literature:

With lithium perchlorate; In tetrahydrofuran; toluene; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1021/jm800613s

Reference yield: 93.0%

tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-nitrophenyl)hydroxyethyl)amino)butylcarbamate (1068147-86-3) + trifluoroacetic acid (76-05-1) → 2-((4-aminobutyl)benzylamino)-1-(4-(benzyloxy)-3-nitrophenyl)ethanol trifluoroacetate (1068147-79-4)

Guidance literature:

In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jm800613s

Reference yield: 47.0%

tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-nitrophenyl)hydroxyethyl)amino)butylcarbamate (1068147-86-3) → tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-aminophenyl)hydroxyethyl)amino)butylcarbamate (1068147-99-8)

Guidance literature:

With platinum(IV) oxide; hydrogen; In methanol; under 760.051 Torr;

DOI:10.1021/jm800613s

upstream raw materials:

N⁽¹⁾-benzyl-N⁽⁴⁾-(tert-butyloxycarbonyl)-1,4-diaminobutane

2-(3-benzyloxy-4-nitrophenyl)oxirane

Downstream raw materials:

tert-butyl 4-(benzyl(2-(4-(benzyloxy)-3-aminophenyl)hydroxyethyl)amino)butylcarbamate

2-((4-aminobutyl)benzylamino)-1-(4-(benzyloxy)-3-nitrophenyl)ethanol trifluoroacetate

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