4,5,9,10-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-diepisulfano-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

Base Information

• Chemical Name: 4,5,9,10-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-diepisulfano-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole
• CAS No.: 24810-25-1
• Molecular Formula: C₃₂H₂₀N₄S₄
• Molecular Weight: 588.802

Synonyms:4,5,9,10-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-diepisulfano-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

Chemical Property of 4,5,9,10-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-diepisulfano-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

Chemical Property:

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Technology Process of 4,5,9,10-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-diepisulfano-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole

There total 2 articles about 4,5,9,10-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-diepisulfano-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C,C'-diphenyl-C,C'-[1,2,5]thiadiazole-3,4-diyl-bis-methanone (72234-52-7) → 4,5,9,10-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-diepisulfano-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole (24810-25-1)

Guidance literature:

Multi-step reaction with 2 steps

1: P₂S₅ / dioxane

2: CH₂Cl₂ / Irradiation

With tetraphosphorus decasulfide; In 1,4-dioxane; dichloromethane;

DOI:10.1021/ja01052a082

Reference yield:

4,6-diphenylthieno<3,4-c><1,2,5>thiadiazole (24793-25-7,24793-62-2) → 4,5,9,10-tetraphenyl-4,5,9,10-tetrahydro-4r,10c;5t,9t-diepisulfano-cycloocta[1,2-c;5,6-c']bis[1,2,5]thiadiazole (24810-25-1)

Guidance literature:

In dichloromethane; Irradiation;

DOI:10.1021/ja01052a082

upstream raw materials:

4,6-diphenylthieno<3,4-c><1,2,5>thiadiazole

C,C'-diphenyl-C,C'-[1,2,5]thiadiazole-3,4-diyl-bis-methanone

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