Technology Process of C24H19F3N2O2
There total 8 articles about C24H19F3N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
copper diacetate;
In
dichloromethane;
at 20 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide; water / ethanol / 3 h / 20 °C
1.2: pH 7 buffer
2.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 16 h / 20 °C
3.1: sodium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 1 h / 20 °C
4.1: pyridine / copper diacetate / dichloromethane / 16 h / 20 °C
With
pyridine; water; sodium hexamethyldisilazane; N-ethyl-N,N-diisopropylamine; HATU; sodium hydroxide;
copper diacetate;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine; formic acid / palladium 10% on activated carbon / ethanol / 2 h / Inert atmosphere
2: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 16 h / 20 °C
3: sodium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 1 h / 20 °C
4: pyridine / copper diacetate / dichloromethane / 16 h / 20 °C
With
pyridine; formic acid; sodium hexamethyldisilazane; triethylamine; N-ethyl-N,N-diisopropylamine; HATU;
palladium 10% on activated carbon; copper diacetate;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;