(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-{2-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-ylsulfanyl]-ethyl} ester 1-(1-methyl-1-phenyl-ethyl) ester

Base Information

Chemical Name:(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-{2-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-ylsulfanyl]-ethyl} ester 1-(1-methyl-1-phenyl-ethyl) ester
CAS No.:207306-00-1
Molecular Formula:C₃₉H₃₇NO₆S₈
Molecular Weight:872.254
Hs Code.:

(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-{2-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-ylsulfanyl]-ethyl} ester 1-(1-methyl-1-phenyl-ethyl) ester

Synonyms:(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-{2-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-ylsulfanyl]-ethyl} ester 1-(1-methyl-1-phenyl-ethyl) ester

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Chemical Property of (S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-{2-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-ylsulfanyl]-ethyl} ester 1-(1-methyl-1-phenyl-ethyl) ester

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Technology Process of (S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-{2-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-ylsulfanyl]-ethyl} ester 1-(1-methyl-1-phenyl-ethyl) ester

There total 6 articles about (S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-{2-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-ylsulfanyl]-ethyl} ester 1-(1-methyl-1-phenyl-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 199729-53-8
4-(2-hydroxyethylthio)-5-methylthio-4',5'-ethylenedithiotetrathiafulvalene

: 207305-95-1
(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 1-(1-methyl-1-phenyl-ethyl) ester

: 207306-00-1
(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-{2-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-ylsulfanyl]-ethyl} ester 1-(1-methyl-1-phenyl-ethyl) ester

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; Ambient temperature;
DOI:10.1039/a800759d

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 207306-00-1
(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-{2-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-ylsulfanyl]-ethyl} ester 1-(1-methyl-1-phenyl-ethyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / Na₂CO₃ / H₂O; dioxane / Ambient temperature

2: 97 percent / cyclohexane; CH₂Cl₂ / Ambient temperature

3: 82 percent / N-methylmorpholine, glacial acetic acid / Pd(PPh₃)4 / CHCl₃ / Ambient temperature

4: 76 percent / diisopropyl azodicarboxylate, PPh₃ / tetrahydrofuran / Ambient temperature

With 4-methyl-morpholine; di-isopropyl azodicarboxylate; sodium carbonate; acetic acid; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; cyclohexane; water;
DOI:10.1039/a800759d

Reference yield:

: 146982-24-3
N-alpha-(9-fluorenylmethyloxycarbonyl)-L-aspartic acid beta-allyl ester

: 207306-00-1
(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-succinic acid 4-{2-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-ylsulfanyl]-ethyl} ester 1-(1-methyl-1-phenyl-ethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / cyclohexane; CH₂Cl₂ / Ambient temperature

2: 82 percent / N-methylmorpholine, glacial acetic acid / Pd(PPh₃)4 / CHCl₃ / Ambient temperature

3: 76 percent / diisopropyl azodicarboxylate, PPh₃ / tetrahydrofuran / Ambient temperature

With 4-methyl-morpholine; di-isopropyl azodicarboxylate; acetic acid; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; chloroform; cyclohexane;
DOI:10.1039/a800759d