(1H-Benzimidazol-2-yl)-piperidin-4-yl-amine 2HBr

Base Information

Chemical Name:(1H-Benzimidazol-2-yl)-piperidin-4-yl-amine 2HBr
CAS No.:75970-47-7
Molecular Formula:C12H16 N4 . 2 Br H
Molecular Weight:0
Hs Code.:
Mol file:75970-47-7.mol

Synonyms:1H-Benzimidazol-2-amine,N-4-piperidinyl-, dihydrobromide (9CI)

Suppliers and Price of (1H-Benzimidazol-2-yl)-piperidin-4-yl-amine 2HBr

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(1H-BENZIMIDAZOL-2-YL)-PIPERIDIN-4-YL-AMINE DIHYDROBROMIDE 95.00%
5MG
$ 500.36

Total 1 raw suppliers

Chemical Property of (1H-Benzimidazol-2-yl)-piperidin-4-yl-amine 2HBr

Chemical Property:

Vapor Pressure:1.48E-09mmHg at 25°C
Boiling Point:475°C at 760 mmHg
Flash Point:241.1°C
PSA：55.97000
LogP:3.39370

Purity/Quality:: (1H-BENZIMIDAZOL-2-YL)-PIPERIDIN-4-YL-AMINE DIHYDROBROMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (1H-Benzimidazol-2-yl)-piperidin-4-yl-amine 2HBr

There total 4 articles about (1H-Benzimidazol-2-yl)-piperidin-4-yl-amine 2HBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 73734-07-3
(1H-benzimidazol-2-yl)-(1-ethoxycarbonyl-piperidin-4-yl)amine

: 75970-47-7
(1H-benzimidazol-2-yl)-(4-piperidinyl)amine dihydrobromide

Guidance literature:: With hydrogen bromide; for 2h; Reflux;
DOI:10.1002/cmdc.201300172

Reference yield:

: 58859-46-4
ethyl 4-aminopiperidine-1-carboxylate

: 75970-47-7
(1H-benzimidazol-2-yl)-(4-piperidinyl)amine dihydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / water / 1 h / 5 °C

1.2: 2 h / 60 - 70 °C

2.1: ethanol / 20 °C

3.1: mercury(II) oxide / ethanol / 2 h / Reflux

4.1: hydrogen bromide / 2 h / Reflux

With hydrogen bromide; mercury(II) oxide; sodium hydroxide; In ethanol; water;
DOI:10.1002/cmdc.201300172

Reference yield:

: 73733-70-7
ethyl 4-isothiocyanato-1-piperidinecarboxylate

: 75970-47-7
(1H-benzimidazol-2-yl)-(4-piperidinyl)amine dihydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 20 °C

2: mercury(II) oxide / ethanol / 2 h / Reflux

3: hydrogen bromide / 2 h / Reflux

With hydrogen bromide; mercury(II) oxide; In ethanol;
DOI:10.1002/cmdc.201300172