2′-amino-N⁶-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

Base Information

Chemical Name:2′-amino-N⁶-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine
CAS No.:1452385-16-8
Molecular Formula:C₂₉H₄₆N₆O₄Si₂
Molecular Weight:598.893
Hs Code.:

2′-amino-N<sup>6</sup>-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

Synonyms:2′-amino-N⁶-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2′-amino-N⁶-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

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Technology Process of 2′-amino-N⁶-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

There total 1 articles about 2′-amino-N⁶-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1245200-31-0
6-N-benzoyl-2′-azido-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

: 1452385-16-8
2′-amino-N⁶-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

Guidance literature:: With hydrogen; In methanol; at 20 ℃; for 12h; under 760.051 Torr;
DOI:10.1039/c3ob41206g

Reference yield: 80.0%

: 1452385-16-8
2′-amino-N⁶-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

: 5231-87-8
3,4-diethoxy-3-cyclobuten-1,2-dione

: N-(9-((2R,3R,4S,5R)-4-((tert-butyldimethylsilyl)oxy)-5-(((tert-butyldimethylsilyl)oxy)methyl)-3-((2-ethoxy-3,4-dioxocyclobut-1-en-1-yl)amino)tetrahydrofuran-2-yl)-9H-purin-6-yl)benzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; at 20 ℃;
DOI:10.1002/anie.201606843

Reference yield:

: 15761-38-3
L-N-Boc-Ala

: 1452385-16-8
2′-amino-N⁶-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

: 1452385-19-1
N⁶-benzoyl-3′,5′-bis-O-(tert-butyl-dimethylsilyl)-2′-(S)-methylcarbamate2′-deoxyadenosine

Guidance literature:: L-N-Boc-Ala; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 0.25h;

2′-amino-N⁶-benzoyl-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1039/c3ob41206g