2,3-epoxycinnamaldehyde dimethyl acetal

Base Information

• Chemical Name: 2,3-epoxycinnamaldehyde dimethyl acetal
• CAS No.: 20202-28-2
• Molecular Formula: C₁₁H₁₄O₃
• Molecular Weight: 194.23
• Mol file: 20202-28-2.mol

Synonyms:2,3-epoxycinnamaldehyde dimethyl acetal

Chemical Property of 2,3-epoxycinnamaldehyde dimethyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-epoxycinnamaldehyde dimethyl acetal

There total 3 articles about 2,3-epoxycinnamaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(E)-3-phenylpropenal (14371-10-9) + methyl iodide (74-88-4) → 2,3-epoxycinnamaldehyde dimethyl acetal (20202-28-2)

Guidance literature:

With 18-crown-6 ether; In toluene;

DOI:10.1016/0040-4020(95)00274-C

Reference yield:

(E)-cinnamaldehyde dimethylacetal (4364-06-1) → Methyl cinnamate (103-26-4,1754-62-7) + 2,3-epoxycinnamaldehyde dimethyl acetal (20202-28-2)

Guidance literature:

With potassium fluoride; sodium fluoride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1.) 15 h, RT; 2.) 1 h, RT;

DOI:10.1246/cl.1983.971

Reference yield:

cinnamaldehyde dimethylacetal (4364-06-1) → 1,2-epoxy-3,3-dimethoxy-1-phenylpropane (20202-28-2,111671-30-8)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 42h; Ambient temperature;

upstream raw materials:

cinnamaldehyde dimethylacetal

(E)-cinnamaldehyde dimethylacetal

(E)-3-phenylpropenal

methyl iodide

Downstream raw materials:

Phenylredukton-1-(4-phenyl-anil)

Phenylredukton-1-(2-nitro-anil)

Phenylredukton-1-(4-methyl-anil)

Phenylredukton-1-(4-nitro-2-methoxy-anil)