C₁₇H₂₃NO₄

Base Information

• Chemical Name: C₁₇H₂₃NO₄
• CAS No.: 1331858-86-6
• Molecular Formula: C₁₇H₂₃NO₄
• Molecular Weight: 305.374
• Mol file: 1331858-86-6.mol

Synonyms:C₁₇H₂₃NO₄

Chemical Property of C₁₇H₂₃NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₃NO₄

There total 3 articles about C₁₇H₂₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-iodo-propane (75-30-9) + isopropyl 3,4-dimethoxyphenylcyanoacetate (1331858-89-9) → C17H23NO4 (1331858-86-6)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ja205717f

Reference yield:

4-Bromoveratrole (2859-78-1) → C17H23NO4 (1331858-86-6)

Guidance literature:

Multi-step reaction with 2 steps

1: tri-tert-butyl phosphine; sodium phosphate; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / toluene / 12 h / 100 °C

2: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C / Inert atmosphere

With tri-tert-butyl phosphine; potassium carbonate; sodium phosphate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In dimethyl sulfoxide; toluene;

DOI:10.1021/ja205717f

Reference yield:

isopropyl cyanoacetate (13361-30-3) → C17H23NO4 (1331858-86-6)

Guidance literature:

Multi-step reaction with 2 steps

1: tri-tert-butyl phosphine; sodium phosphate; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / toluene / 12 h / 100 °C

2: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C / Inert atmosphere

With tri-tert-butyl phosphine; potassium carbonate; sodium phosphate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In dimethyl sulfoxide; toluene;

DOI:10.1021/ja205717f

upstream raw materials:

2-iodo-propane

isopropyl 3,4-dimethoxyphenylcyanoacetate

isopropyl cyanoacetate

4-Bromoveratrole

Downstream raw materials:

γ-Cyano-γ-3,4-dimethoxyphenyl-γ-isopropyl-1-buten