(2S)-2-tert-butoxycarbonylamino-3-hydroxy-2-methylpropionic acid 2-(4-octyl-phenyl)-2-oxo-ethyl ester

Base Information

• Chemical Name: (2S)-2-tert-butoxycarbonylamino-3-hydroxy-2-methylpropionic acid 2-(4-octyl-phenyl)-2-oxo-ethyl ester
• CAS No.: 1190087-34-3
• Molecular Formula: C₂₅H₃₉NO₆
• Molecular Weight: 449.588

Synonyms:(2S)-2-tert-butoxycarbonylamino-3-hydroxy-2-methylpropionic acid 2-(4-octyl-phenyl)-2-oxo-ethyl ester

Chemical Property of (2S)-2-tert-butoxycarbonylamino-3-hydroxy-2-methylpropionic acid 2-(4-octyl-phenyl)-2-oxo-ethyl ester

Chemical Property:

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Technology Process of (2S)-2-tert-butoxycarbonylamino-3-hydroxy-2-methylpropionic acid 2-(4-octyl-phenyl)-2-oxo-ethyl ester

There total 1 articles about (2S)-2-tert-butoxycarbonylamino-3-hydroxy-2-methylpropionic acid 2-(4-octyl-phenyl)-2-oxo-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

α-bromomethyl p(n-octyl)phenyl cetone (64068-76-4) + (S)-2-tert-Butoxycarbonylamino-3-hydroxy-2-methyl-propionic acid (84311-19-3) → (2S)-2-tert-butoxycarbonylamino-3-hydroxy-2-methylpropionic acid 2-(4-octyl-phenyl)-2-oxo-ethyl ester (1190087-34-3)

Guidance literature:

(S)-2-tert-Butoxycarbonylamino-3-hydroxy-2-methyl-propionic acid; With caesium carbonate; In ethanol; Sonication;

α-bromomethyl p(n-octyl)phenyl cetone; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.bmc.2009.04.015

Reference yield:

(2S)-2-tert-butoxycarbonylamino-3-hydroxy-2-methylpropionic acid 2-(4-octyl-phenyl)-2-oxo-ethyl ester (1190087-34-3) → (2R)-{2-hydroxy-1-methyl-1-[5-(4-octyl-phenyl)-1H-imidazol-2-yl]-ethyl}-carbamic acid tert-butyl ester (1190087-35-4)

Guidance literature:

With ammonium acetate; In 5,5-dimethyl-1,3-cyclohexadiene; at 110 - 120 ℃;

DOI:10.1016/j.bmc.2009.04.015

upstream raw materials:

α-bromomethyl p(n-octyl)phenyl cetone

(S)-2-tert-Butoxycarbonylamino-3-hydroxy-2-methyl-propionic acid

Downstream raw materials:

(2R)-{2-hydroxy-1-methyl-1-[5-(4-octyl-phenyl)-1H-imidazol-2-yl]-ethyl}-carbamic acid tert-butyl ester

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