1,7-bis(3,5-di-tert-butylphenyl)-N,N'-dioctyl-3:4,9:10-perylenetetracarboxydiimide

Base Information

Chemical Name:1,7-bis(3,5-di-tert-butylphenyl)-N,N'-dioctyl-3:4,9:10-perylenetetracarboxydiimide
CAS No.:1379575-19-5
Molecular Formula:C₆₈H₈₂N₂O₄
Molecular Weight:991.41
Hs Code.:

Synonyms:1,7-bis(3,5-di-tert-butylphenyl)-N,N'-dioctyl-3:4,9:10-perylenetetracarboxydiimide

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Chemical Property of 1,7-bis(3,5-di-tert-butylphenyl)-N,N'-dioctyl-3:4,9:10-perylenetetracarboxydiimide

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Technology Process of 1,7-bis(3,5-di-tert-butylphenyl)-N,N'-dioctyl-3:4,9:10-perylenetetracarboxydiimide

There total 2 articles about 1,7-bis(3,5-di-tert-butylphenyl)-N,N'-dioctyl-3:4,9:10-perylenetetracarboxydiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 209111-67-1
N,N'-bis(n-octyl)-1,7-dibromo-perylene-3,4:9,10-bis(dicarboximide)

: 197223-39-5
3,5-di-tert-butylphenyl boronic acid

: 1379575-19-5
1,7-bis(3,5-di-tert-butylphenyl)-N,N'-dioctyl-3:4,9:10-perylenetetracarboxydiimide

Guidance literature:: N,N'-bis(n-octyl)-1,7-dibromo-perylene-3,4:9,10-bis(dicarboximide); 3,5-di-tert-butylphenyl boronic acid; With dichloro[1,1'-bis(di-t-butylphosphino)ferrocene]palladium(II); In water; at 20 ℃; for 0.0833333h;

With triethylamine; In water; at 80 ℃; for 12h;
DOI:10.1016/j.jorganchem.2022.122267

Reference yield:

: 1,6-dibromo-N,N'-di(2-ethylhexyl)-perylene-3,4,9,10-tetracarboxydiimide

: 1071924-13-4
2-[3,5-bis(1,1-dimethylethyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 209111-67-1
N,N'-bis(n-octyl)-1,7-dibromo-perylene-3,4:9,10-bis(dicarboximide)

: 1379575-19-5
1,7-bis(3,5-di-tert-butylphenyl)-N,N'-dioctyl-3:4,9:10-perylenetetracarboxydiimide

: 1379575-20-8
1,6-bis(3,5-di-tert-butylphenyl)-N,N'-dioctyl-3:4,9:10-perylenetetracarboxydiimide

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; tetrabutyl-ammonium chloride; potassium carbonate; In water; toluene; at 90 ℃; for 22h; regiospecific reaction; Inert atmosphere;
DOI:10.1002/ejoc.201101825