Al(C₆H₂(C(CH₃)3)2(CH₃)O)2(OCH(C₆H₅)2)(OC(C₆H₅)2)

Base Information

Chemical Name:Al(C₆H₂(C(CH₃)3)2(CH₃)O)2(OCH(C₆H₅)2)(OC(C₆H₅)2)
CAS No.:140463-76-9
Molecular Formula:C₅₆H₆₇AlO₄
Molecular Weight:831.127
Hs Code.:

Al(C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)2(CH<sub>3</sub>)O)2(OCH(C<sub>6</sub>H<sub>5</sub>)2)(OC(C<sub>6</sub>H<sub>5</sub>)2)

Synonyms:Al(C₆H₂(C(CH₃)3)2(CH₃)O)2(OCH(C₆H₅)2)(OC(C₆H₅)2)

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Chemical Property of Al(C₆H₂(C(CH₃)3)2(CH₃)O)2(OCH(C₆H₅)2)(OC(C₆H₅)2)

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Technology Process of Al(C₆H₂(C(CH₃)3)2(CH₃)O)2(OCH(C₆H₅)2)(OC(C₆H₅)2)

There total 5 articles about Al(C₆H₂(C(CH₃)3)2(CH₃)O)2(OCH(C₆H₅)2)(OC(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 61986-88-7
aluminum(ethyl)(2,6-di-tert-butyl-4-methylphenoxy)2

: 140463-76-9
Al(C₆H₂(C(CH₃)3)2(CH₃)O)2(OCH(C₆H₅)2)(OC(C₆H₅)2)

Guidance literature:: With benzophenone; In pentane; byproducts: C2H4; dropwise addn. of 2 equiv of benzophenone in pentane to a soln. of AlEt(BHT)2 in pentane under N2, color change to deep red, stirring (1 h), pptn.; filtration, drying (vac.), further crop by concg. the filtrate, cooling (-20°C, overnight), recrystn. (hexane); elem. anal.;
DOI:10.1021/om00041a017

Reference yield: 75.0%

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

: 97-93-8
triethylaluminum

: Al(C₂H₅)(C₆H₂(C(CH₃)3)2(CH₃)O)(OCH(C₆H₅)2)(OC(C₆H₅)2)

: 140463-76-9
Al(C₆H₂(C(CH₃)3)2(CH₃)O)2(OCH(C₆H₅)2)(OC(C₆H₅)2)

Guidance literature:: With benzophenone; In pentane; addn. of AlEt3 in hexanes via syringe to a soln. of the phenol in pentane under N2, stirring (0.5 h), dropwise addn. of benzophenone, stirring (1 h), pptn.; filtration, washing (pentane), drying (vac.);
DOI:10.1021/om00041a017

Reference yield:

: Al(C₂H₅)(C₆H₂(C(CH₃)3)2(CH₃)O)2(OC(C₆H₅)2)

: 140463-76-9
Al(C₆H₂(C(CH₃)3)2(CH₃)O)2(OCH(C₆H₅)2)(OC(C₆H₅)2)

Guidance literature:: With benzophenone; In ⁽²⁾H₈-toluene; byproducts: C2H4; heating excess benzophenone with AlEt(BHT)2(OCPh2) in toluene-d8 in a NMR tube at 292-316 K under N2; not isolated; detected by 1H-NMR; Kinetics;
DOI:10.1021/om00041a017