cyclohexyl 2-pyridinesulfonate

Base Information

Chemical Name:cyclohexyl 2-pyridinesulfonate
CAS No.:117800-88-1
Molecular Formula:C₁₁H₁₅NO₃S
Molecular Weight:241.311
Hs Code.:

Synonyms:cyclohexyl 2-pyridinesulfonate

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Chemical Property of cyclohexyl 2-pyridinesulfonate

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Technology Process of cyclohexyl 2-pyridinesulfonate

There total 2 articles about cyclohexyl 2-pyridinesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 66715-65-9
pyridine-2-sulfonyl chloride

: 108-93-0
cyclohexanol

: 117800-88-1
cyclohexyl 2-pyridinesulfonate

Guidance literature:: With triethylamine; at 2 ℃; for 3h;
DOI:10.1021/jo00263a024

Reference yield:

: 2637-34-5,73018-10-7
2-Sulfanylpyridine

: 117800-88-1
cyclohexyl 2-pyridinesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / Cl₂, aq. HCl / 0.5 h / 5 °C

2: 85 percent / triethylamine / 3 h / 2 °C

With hydrogenchloride; chlorine; triethylamine;
DOI:10.1021/jo00263a024

Reference yield: 81.0%

: 117800-88-1
cyclohexyl 2-pyridinesulfonate

: 52200-47-2
2-(cyclohexyloxy)pyridine

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium tert-butylate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride; In 5,5-dimethyl-1,3-cyclohexadiene; at 140 ℃; for 1h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.9b02858