(S)-3-(4-benzyloxybenzenesulfonylamino)-N-hydroxy-2-piperidin-1-ylpropionamide

Base Information

Chemical Name:(S)-3-(4-benzyloxybenzenesulfonylamino)-N-hydroxy-2-piperidin-1-ylpropionamide
CAS No.:1260144-10-2
Molecular Formula:C₂₁H₂₇N₃O₅S
Molecular Weight:433.528
Hs Code.:

Synonyms:(S)-3-(4-benzyloxybenzenesulfonylamino)-N-hydroxy-2-piperidin-1-ylpropionamide

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Chemical Property of (S)-3-(4-benzyloxybenzenesulfonylamino)-N-hydroxy-2-piperidin-1-ylpropionamide

Chemical Property:

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Technology Process of (S)-3-(4-benzyloxybenzenesulfonylamino)-N-hydroxy-2-piperidin-1-ylpropionamide

There total 6 articles about (S)-3-(4-benzyloxybenzenesulfonylamino)-N-hydroxy-2-piperidin-1-ylpropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1260144-14-6
(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid

: 1260144-10-2
(S)-3-(4-benzyloxybenzenesulfonylamino)-N-hydroxy-2-piperidin-1-ylpropionamide

Guidance literature:: (S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 0.333333h;

With O-(tert-butyldimethylsilanyl)hydroxylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

With sodium hydrogencarbonate; In water; N,N-dimethyl-formamide; for 0.333333h;

Reference yield:

: 825-90-1
sodium p-hydroxybenzenesulfonate

: 1260144-10-2
(S)-3-(4-benzyloxybenzenesulfonylamino)-N-hydroxy-2-piperidin-1-ylpropionamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / isopropyl alcohol; water / 20 h / 70 °C

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 18 h / -20 - 20 °C

3.1: triethylamine / dichloromethane / 18 h / 20 °C

4.1: water; lithium hydroxide / tetrahydrofuran / 18 h / 20 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.33 h

5.2: 18 h / 20 °C

5.3: 0.33 h

With oxalyl dichloride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 111712-04-0
4-phenylmethoxybenzenesulfonic acid sodium salt

: 1260144-10-2
(S)-3-(4-benzyloxybenzenesulfonylamino)-N-hydroxy-2-piperidin-1-ylpropionamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 18 h / -20 - 20 °C

2.1: triethylamine / dichloromethane / 18 h / 20 °C

3.1: water; lithium hydroxide / tetrahydrofuran / 18 h / 20 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.33 h

4.2: 18 h / 20 °C

4.3: 0.33 h

With oxalyl dichloride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;