(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid

Base Information

Chemical Name:(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid
CAS No.:1260144-14-6
Molecular Formula:C₂₁H₂₆N₂O₅S
Molecular Weight:418.514
Hs Code.:

Synonyms:(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid

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Chemical Property of (S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid

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Technology Process of (S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid

There total 5 articles about (S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1260144-13-5
methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

: 1260144-14-6
(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid

Guidance literature:: methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate; With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 18h;

With acetic acid; In water;

Reference yield:

: 111712-04-0
4-phenylmethoxybenzenesulfonic acid sodium salt

: 1260144-14-6
(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 18 h / -20 - 20 °C

2: triethylamine / dichloromethane / 18 h / 20 °C

3: water; lithium hydroxide / tetrahydrofuran / 18 h / 20 °C

With oxalyl dichloride; water; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 87001-32-9
p-benzyloxybenzenesulfonyl chloride

: 1260144-14-6
(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 18 h / 20 °C

2: water; lithium hydroxide / tetrahydrofuran / 18 h / 20 °C

With water; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane;