6-N-benzoyl-5'-O-toluoyl-2',3'-O-cyclic adenylic acid n-tetrabutylammonium salt

Base Information

• Chemical Name: 6-N-benzoyl-5'-O-toluoyl-2',3'-O-cyclic adenylic acid n-tetrabutylammonium salt
• CAS No.: 128060-39-9
• Molecular Formula: C₁₆H₃₆N*C₂₅H₂₁N₅O₈P
• Molecular Weight: 792.913

Synonyms:6-N-benzoyl-5'-O-toluoyl-2',3'-O-cyclic adenylic acid n-tetrabutylammonium salt

Chemical Property of 6-N-benzoyl-5'-O-toluoyl-2',3'-O-cyclic adenylic acid n-tetrabutylammonium salt

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Technology Process of 6-N-benzoyl-5'-O-toluoyl-2',3'-O-cyclic adenylic acid n-tetrabutylammonium salt

There total 3 articles about 6-N-benzoyl-5'-O-toluoyl-2',3'-O-cyclic adenylic acid n-tetrabutylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

C51H55N7O16PSSi(1-)*C6H15N(1+) (128060-60-6) → C45H41N7O16PS(1-)*C6H15N(1+) (128060-62-8) + Acetic acid (2R,3R,4S,5S)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester (128060-35-5) + Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester (128090-32-4) + 6-N-benzoyl-5'-O-toluoyl-2',3'-O-cyclic adenylic acid n-tetrabutylammonium salt (128060-39-9)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1016/S0040-4020(01)89215-2

Reference yield: 11.0%

C45H41N7O16PS(1-)*C6H15N(1+) (128060-62-8) → Acetic acid (2R,3R,4S,5S)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester (128060-35-5) + Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester (128090-32-4) + 6-N-benzoyl-5'-O-toluoyl-2',3'-O-cyclic adenylic acid n-tetrabutylammonium salt (128060-39-9)

Guidance literature:

With silica gel; In water; acetonitrile; at 40 ℃; for 96h;

DOI:10.1016/S0040-4020(01)89215-2

Reference yield: 11.0%

6-N-benzoyl-2'-O-pixyl-5'-O-toluoyladenosine-3'-phosphoromonofluoridate n-tetrabutylammonium salt (128060-37-7) → 6-N-benzoyl-5'-O-toluoyl-2',3'-O-cyclic adenylic acid n-tetrabutylammonium salt (128060-39-9) + 2'-(6-N-benzoyl-5'-O-toluoyl)adenylic acid n-tetrabutylammonium salt (128060-43-5) + 3'-(6-N-benzoyl-5'-O-toluoyl)adenylic acid n-tetrabutylammonium salt (128060-41-3)

Guidance literature:

With acetic acid; at 20 ℃; for 0.5h; Yields of byproduct given;

DOI:10.1016/S0040-4020(01)89215-2

upstream raw materials:

6-N-benzoyl-2'-O-pixyl-5'-O-toluoyladenosine-3'-phosphoromonofluoridate n-tetrabutylammonium salt

C₄₅H₄₁N₇O₁₆PS^(1-)*C₆H₁₅N⁽¹⁺⁾

C₅₁H₅₅N₇O₁₆PSSi^(1-)*C₆H₁₅N⁽¹⁺⁾

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