Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester

Base Information

• Chemical Name: Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester
• CAS No.: 128090-32-4
• Molecular Formula: C₄₀H₃₈N₄O₁₆S₂
• Molecular Weight: 894.891

Synonyms:Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester

Chemical Property of Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester

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Technology Process of Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester

There total 8 articles about Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

C70H57ClN7O17PS (128060-30-0,128112-17-4) + tetra-n-butylammoniumfluoride trihydrate (22206-57-1,153005-55-1) → 6-N-benzoyl-2'-O-pixyl-5'-O-toluoyladenosine-3'-phosphoromonofluoridate n-tetrabutylammonium salt (128060-37-7) + Acetic acid (2R,3R,4S,5S)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-benzoylsulfanylmethyl-tetrahydro-furan-3-yl ester (128060-33-3) + Acetic acid (2R,3R,4S,5S)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester (128060-35-5) + Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester (128090-32-4)

Guidance literature:

In tetrahydrofuran; pyridine; water; at 20 ℃; for 1h; Further byproducts given;

DOI:10.1016/S0040-4020(01)89215-2

Reference yield: 58.0%

C51H55N7O16PSSi(1-)*C6H15N(1+) (128060-60-6) → C45H41N7O16PS(1-)*C6H15N(1+) (128060-62-8) + Acetic acid (2R,3R,4S,5S)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester (128060-35-5) + Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester (128090-32-4) + 6-N-benzoyl-5'-O-toluoyl-2',3'-O-cyclic adenylic acid n-tetrabutylammonium salt (128060-39-9)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1016/S0040-4020(01)89215-2

Reference yield: 44.0%

C64H53N7O17PS(1-)*C6H15N(1+) (128060-58-2) → C45H41N7O16PS(1-)*C6H15N(1+) (128060-62-8) + Acetic acid (2R,3R,4S,5S)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester (128060-35-5) + Acetic acid (2S,3S,4R,5R)-4-acetoxy-2-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-5-[(2S,3S,4R,5R)-3,4-diacetoxy-5-(3-benzoyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyldisulfanylmethyl]-tetrahydro-furan-3-yl ester (128090-32-4)

Guidance literature:

With acetic acid; at 20 ℃; for 0.5h;

DOI:10.1016/S0040-4020(01)89215-2

upstream raw materials:

C₇₀H₅₇ClN₇O₁₇PS

tetra-n-butylammoniumfluoride trihydrate

C₄₅H₄₁N₇O₁₆PS^(1-)*C₆H₁₅N⁽¹⁺⁾

C₅₁H₅₅N₇O₁₆PSSi^(1-)*C₆H₁₅N⁽¹⁺⁾

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