2-(N,N-diphenylcarbamoyloxymethyl)-5-ethoxycarbonylmethyloxy-3,4-dihydronaphthalene

Base Information

Chemical Name:2-(N,N-diphenylcarbamoyloxymethyl)-5-ethoxycarbonylmethyloxy-3,4-dihydronaphthalene
CAS No.:172936-75-3
Molecular Formula:C₂₈H₂₇NO₅
Molecular Weight:457.526
Hs Code.:

Synonyms:2-(N,N-diphenylcarbamoyloxymethyl)-5-ethoxycarbonylmethyloxy-3,4-dihydronaphthalene

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Chemical Property of 2-(N,N-diphenylcarbamoyloxymethyl)-5-ethoxycarbonylmethyloxy-3,4-dihydronaphthalene

Chemical Property:

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Technology Process of 2-(N,N-diphenylcarbamoyloxymethyl)-5-ethoxycarbonylmethyloxy-3,4-dihydronaphthalene

There total 5 articles about 2-(N,N-diphenylcarbamoyloxymethyl)-5-ethoxycarbonylmethyloxy-3,4-dihydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 172938-01-1
5-t-butyldiphenylsilyloxy-2-hydroxymethyl-3,4-dihydronaphthalene

: 172936-75-3
2-(N,N-diphenylcarbamoyloxymethyl)-5-ethoxycarbonylmethyloxy-3,4-dihydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: tetrabutylammonium fluoride / tetrahydrofuran

3: K₂CO₃ / dimethylformamide

With pyridine; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.04.047

Reference yield:

: 172937-64-3
2-ethoxycarbonyl-5-t-butyldiphenylsilyloxy-3,4-dihydronaphthalene

: 172936-75-3
2-(N,N-diphenylcarbamoyloxymethyl)-5-ethoxycarbonylmethyloxy-3,4-dihydronaphthalene

Guidance literature:: Multi-step reaction with 4 steps

1: DIBAL-H / toluene

2: pyridine

3: tetrabutylammonium fluoride / tetrahydrofuran

4: K₂CO₃ / dimethylformamide

With pyridine; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2005.04.047

Reference yield:

: 172937-63-2
1-hydroxy-2-ethoxycarbonyl-5-t-butyldiphenylsilyloxy-1,2,3,4-tetrahydronaphthalene

: 172936-75-3
2-(N,N-diphenylcarbamoyloxymethyl)-5-ethoxycarbonylmethyloxy-3,4-dihydronaphthalene

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / KHSO₄ / toluene

2: DIBAL-H / toluene

3: pyridine

4: tetrabutylammonium fluoride / tetrahydrofuran

5: K₂CO₃ / dimethylformamide

With pyridine; potassium hydrogensulfate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2005.04.047