Technology Process of C26H30ClN3O4
There total 9 articles about C26H30ClN3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium tert-butylate;
In
N,N-dimethyl acetamide;
at 98 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: iron; ammonium acetate / toluene; water / 105 °C
2.1: sodium methylate / 1,2-dimethoxyethane / 0.5 h / Inert atmosphere
2.2: Inert atmosphere
3.1: trichlorophosphate / 10 h / Reflux
4.1: methanesulfonic acid; trifluoroacetic acid / 3 h / Reflux
4.2: 2 h / pH 7
5.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C
6.1: sodium iodide; potassium carbonate / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere
7.1: potassium tert-butylate / N,N-dimethyl acetamide / 98 °C / Inert atmosphere
With
methanesulfonic acid; potassium tert-butylate; ammonium acetate; sodium methylate; iron; potassium carbonate; trifluoroacetic acid; sodium iodide; trichlorophosphate;
In
1,2-dimethoxyethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium iodide; potassium carbonate / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere
2: potassium tert-butylate / N,N-dimethyl acetamide / 98 °C / Inert atmosphere
With
potassium tert-butylate; potassium carbonate; sodium iodide;
In
N,N-dimethyl acetamide; N,N-dimethyl-formamide;