trifluoro-methanesulfonic acid 6-methanesulfonyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

Base Information

Chemical Name:trifluoro-methanesulfonic acid 6-methanesulfonyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester
CAS No.:651326-69-1
Molecular Formula:C₂₆H₂₆F₃NO₈S₂
Molecular Weight:601.622
Hs Code.:

Synonyms:trifluoro-methanesulfonic acid 6-methanesulfonyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

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Chemical Property of trifluoro-methanesulfonic acid 6-methanesulfonyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

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Technology Process of trifluoro-methanesulfonic acid 6-methanesulfonyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

There total 5 articles about trifluoro-methanesulfonic acid 6-methanesulfonyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 861930-70-3
trifluoro-methanesulfonic acid 6-hydroxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

: 124-63-0
methanesulfonyl chloride

: 651326-69-1
trifluoro-methanesulfonic acid 6-methanesulfonyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.333333h;
DOI:10.1021/jm0509795

Reference yield:

: 649724-98-1
(2-hydroxy-6-methoxy-naphthalen-1-yl)-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-methanone

: 651326-69-1
trifluoro-methanesulfonic acid 6-methanesulfonyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / CH₂Cl₂ / 0.25 h / 0 °C

2: 100 percent / HCl; BBr₃; 2-methylbut-2-ene / diethyl ether; CH₂Cl₂ / 2 h / 0 °C

3: 99 percent / diisopropylethylamine / CH₂Cl₂ / 0.33 h / 20 °C

With pyridine; hydrogenchloride; 2-methyl-but-2-ene; boron tribromide; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jm0509795

Reference yield:

: 5486-55-5,117119-43-4
2,6-dimethoxylnaphthalene

: 651326-69-1
trifluoro-methanesulfonic acid 6-methanesulfonyloxy-1-[4-(2-piperidin-1-yl-ethoxy)-benzoyl]-naphthalen-2-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum chloride / CH₂Cl₂ / -10 - 20 °C

2: 100 percent / pyridine / CH₂Cl₂ / 0.25 h / 0 °C

3: 100 percent / HCl; BBr₃; 2-methylbut-2-ene / diethyl ether; CH₂Cl₂ / 2 h / 0 °C

4: 99 percent / diisopropylethylamine / CH₂Cl₂ / 0.33 h / 20 °C

With pyridine; hydrogenchloride; aluminium trichloride; 2-methyl-but-2-ene; boron tribromide; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jm0509795