(1S,3R,4S)-4-(benzyloxymethyl)-2,2-dichloro-3-((R)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutyl methanesulfonate

Base Information

Chemical Name:(1S,3R,4S)-4-(benzyloxymethyl)-2,2-dichloro-3-((R)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutyl methanesulfonate
CAS No.:1240521-01-0
Molecular Formula:C₃₀H₄₂Cl₂O₅S
Molecular Weight:585.632
Hs Code.:

Synonyms:(1S,3R,4S)-4-(benzyloxymethyl)-2,2-dichloro-3-((R)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutyl methanesulfonate

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Chemical Property of (1S,3R,4S)-4-(benzyloxymethyl)-2,2-dichloro-3-((R)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutyl methanesulfonate

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Technology Process of (1S,3R,4S)-4-(benzyloxymethyl)-2,2-dichloro-3-((R)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutyl methanesulfonate

There total 1 articles about (1S,3R,4S)-4-(benzyloxymethyl)-2,2-dichloro-3-((R)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1240520-83-5
(1S,3R,4R)-4-(benzyloxymethyl)-2,2-dichloro-3-((R)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutanol

: 124-63-0
methanesulfonyl chloride

: 1240521-01-0
(1S,3R,4S)-4-(benzyloxymethyl)-2,2-dichloro-3-((R)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutyl methanesulfonate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol101559b

Reference yield: 87.0%

: 1240521-01-0
(1S,3R,4S)-4-(benzyloxymethyl)-2,2-dichloro-3-((R)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutyl methanesulfonate

: 1240520-92-6
2-((R)-1-((1R,4S)-4-(benzyloxymethyl)-2-chlorocyclobut-2-enyloxy)ethyl)-1,3,5-triisopropylbenzene

Guidance literature:: With zinc/copper couple; ammonium chloride; In methanol; diethyl ether; at 30 - 35 ℃; for 2.41667h; Inert atmosphere; Sonication;
DOI:10.1021/ol101559b