Technology Process of (1,2,5,6-η4-cyclooctadiene)(2,4-dinitrophenyl)(4-nitrophenyl)platinum(II)
There total 1 articles about (1,2,5,6-η4-cyclooctadiene)(2,4-dinitrophenyl)(4-nitrophenyl)platinum(II) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
1,1,2,2-tetrachloroethylene;
stannane added to Pt-complex in CH2Cl2 with stirring, mixt. heated for 24 h at 60°C; solvent removed, chromy. (SiO2, CH2Cl2); soln. layered with petroleum ether, stored for 24 h at -20°C, elem. anal.;
- Guidance literature:
-
With
triphenylphosphine;
In
dichloromethane;
byproducts: 1,5-COD; (Ar); mixt. stirred for 6 h in the dark at room temp.; soln. reduced in volume, layered with petroleum ether, stored for 24 h at -20°C, elem. anal.;