8-[4-(5-aminopyrazin-2-yl)phenyl]-2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

Base Information

Chemical Name:8-[4-(5-aminopyrazin-2-yl)phenyl]-2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene
CAS No.:1207336-31-9
Molecular Formula:C₂₇H₃₀BF₂N₅
Molecular Weight:473.377
Hs Code.:

Synonyms:8-[4-(5-aminopyrazin-2-yl)phenyl]-2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

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Chemical Property of 8-[4-(5-aminopyrazin-2-yl)phenyl]-2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 8-[4-(5-aminopyrazin-2-yl)phenyl]-2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

There total 2 articles about 8-[4-(5-aminopyrazin-2-yl)phenyl]-2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 59489-71-3
5-amino-2-bromopyrazine

: 1207336-30-8
2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-8-[4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenyl]-4-bora-3a,4a-diaza-s-indacene

: 1207336-31-9
8-[4-(5-aminopyrazin-2-yl)phenyl]-2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; for 3h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2009.11.086

Reference yield:

: C₂₇H₃₁N₅

: 1207336-31-9
8-[4-(5-aminopyrazin-2-yl)phenyl]-2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: C₂₇H₃₁N₅; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.333333h; Inert atmosphere;

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.11.086