(S)-3-phenylhexane

Base Information

Chemical Name:(S)-3-phenylhexane
CAS No.:35216-62-7
Molecular Formula:C₁₂H₁₈
Molecular Weight:162.275
Hs Code.:

Synonyms:(S)-3-phenylhexane

Suppliers and Price of (S)-3-phenylhexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-phenylhexane

Chemical Property:

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Technology Process of (S)-3-phenylhexane

There total 14 articles about (S)-3-phenylhexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: Methanesulfonic acid (1S,2R)-1-ethyl-4-methanesulfonyloxy-2-phenyl-butyl ester

: 35216-62-7
(S)-3-phenylhexane

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 100 ℃; for 24h;
DOI:10.1021/jo00059a027

Reference yield:

: 2--4-phenyl-3-butenenitrile

: 35216-62-7
(S)-3-phenylhexane

Guidance literature:: Multi-step reaction with 5 steps

1: 1) LDA, HMPA / 1) THF, -78 deg C, 2) THF, -78 deg C, 1 h

2: aq. oxalic acid / tetrahydrofuran / 12 h / 100 °C

3: 1) BH₃*SMe₂, 2) glycerin, H₂₀ / 1) THF, 100 deg C, 2) THF, reflux

4: Et₃N / CH₂Cl₂

5: LiAlH₄ / tetrahydrofuran / Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; dimethylsulfide borane complex; water; oxalic acid; triethylamine; glycerol; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00059a027