N-phenylcarbonyl-D-norvaline ethyl ester

Base Information

Chemical Name:N-phenylcarbonyl-D-norvaline ethyl ester
CAS No.:197960-69-3
Molecular Formula:C₁₄H₁₉NO₃
Molecular Weight:249.31
Hs Code.:

Synonyms:N-phenylcarbonyl-D-norvaline ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenylcarbonyl-D-norvaline ethyl ester

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Technology Process of N-phenylcarbonyl-D-norvaline ethyl ester

There total 2 articles about N-phenylcarbonyl-D-norvaline ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 144447-82-5
D-norvaline ethyl ester

: 98-88-4
benzoyl chloride

: 197960-69-3
N-phenylcarbonyl-D-norvaline ethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1021/jo970591k

Reference yield:

: 2013-12-9,498-18-0
D-norvaline

: 197960-69-3
N-phenylcarbonyl-D-norvaline ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / thionyl chloride / 10 h / Heating

2: 94 percent / triethylamine / CH₂Cl₂ / 24 h / 0 - 20 °C

With thionyl chloride; triethylamine; In dichloromethane; 1: Esterification / 2: Acylation;
DOI:10.1021/jo970591k