N-{[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)phenyl]-N-[tert-butoxycarbonylsulfamoyl]}acetic acid tert-butyl ester

Base Information

Chemical Name:N-{[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)phenyl]-N-[tert-butoxycarbonylsulfamoyl]}acetic acid tert-butyl ester
CAS No.:952339-05-8
Molecular Formula:C₃₀H₄₆N₂O₈SSi
Molecular Weight:622.855
Hs Code.:

Synonyms:N-{[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)phenyl]-N-[tert-butoxycarbonylsulfamoyl]}acetic acid tert-butyl ester

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Chemical Property of N-{[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)phenyl]-N-[tert-butoxycarbonylsulfamoyl]}acetic acid tert-butyl ester

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Technology Process of N-{[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)phenyl]-N-[tert-butoxycarbonylsulfamoyl]}acetic acid tert-butyl ester

There total 6 articles about N-{[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)phenyl]-N-[tert-butoxycarbonylsulfamoyl]}acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1189-71-5
isocyanate de chlorosulfonyle

: 952339-03-6
[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)-phenylamino]-acetic acid tert-butyl ester

: 952339-05-8
N-{[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)phenyl]-N-[tert-butoxycarbonylsulfamoyl]}acetic acid tert-butyl ester

Guidance literature:: isocyanate de chlorosulfonyle; tert-butyl alcohol; In dichloromethane; at 0 - 20 ℃; for 0.25h;

[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)-phenylamino]-acetic acid tert-butyl ester; With triethylamine; In dichloromethane; at 20 ℃; for 18h;

Reference yield:

: 221615-94-7
3-(benzyloxy)-4-nitrophenol

: 952339-05-8
N-{[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)phenyl]-N-[tert-butoxycarbonylsulfamoyl]}acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole; dmap / N,N-dimethyl-formamide / 18 h

2.1: hydrogen / platinum on carbon / ethyl acetate / 18 h

3.1: potassium carbonate / N,N-dimethyl-formamide / 23 h / 60 °C

4.1: dichloromethane / 0.25 h / 0 - 20 °C

4.2: 18 h / 20 °C

With 1H-imidazole; dmap; hydrogen; potassium carbonate; platinum on carbon; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 952338-99-7
(3-benzyloxy-4-nitrophenoxy)-tert-butyldimethylsilane

: 952339-05-8
N-{[2-benzyloxy-4-(tert-butyldimethylsilanyloxy)phenyl]-N-[tert-butoxycarbonylsulfamoyl]}acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / platinum on carbon / ethyl acetate / 18 h

2.1: potassium carbonate / N,N-dimethyl-formamide / 23 h / 60 °C

3.1: dichloromethane / 0.25 h / 0 - 20 °C

3.2: 18 h / 20 °C

With hydrogen; potassium carbonate; platinum on carbon; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;