Technology Process of benzyl 2-O-benzyl-3-methoxy-4-O-methylgyrophorate
There total 6 articles about benzyl 2-O-benzyl-3-methoxy-4-O-methylgyrophorate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic anhydride;
In
toluene;
for 12h;
DOI:10.1071/C98082
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N,N-dimethylformamide / 24 h / Ambient temperature
2: 85 percent m-chloroperbenzoic acid / CH2Cl2 / 1 h / Ambient temperature
3: potassium carbonate / acetone / 22 h / Heating
4: 69 percent / aq. potassium hydroxide / dimethylsulfoxide / 3 h / 90 °C
5: 22 percent / trifluoroacetic anhydride / toluene / 12 h
With
potassium hydroxide; potassium carbonate; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride;
In
dichloromethane; dimethyl sulfoxide; acetone; toluene;
DOI:10.1071/C98082
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N,N-dimethylformamide / 24 h / Ambient temperature
2: 85 percent m-chloroperbenzoic acid / CH2Cl2 / 1 h / Ambient temperature
3: potassium carbonate / acetone / 22 h / Heating
4: 69 percent / aq. potassium hydroxide / dimethylsulfoxide / 3 h / 90 °C
5: 22 percent / trifluoroacetic anhydride / toluene / 12 h
With
potassium hydroxide; potassium carbonate; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride;
In
dichloromethane; dimethyl sulfoxide; acetone; toluene;
DOI:10.1071/C98082
