N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide

Base Information

Chemical Name:N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide
CAS No.:1429347-23-8
Molecular Formula:C₂₂H₂₉N₅O₃S
Molecular Weight:443.57
Hs Code.:

Synonyms:N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide

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Chemical Property of N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide

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Technology Process of N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide

There total 6 articles about N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1429347-66-9
N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2-trityl-2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide

: 1429347-23-8
N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide

Guidance literature:: N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2-trityl-2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide; With hydrogenchloride; In isopropyl alcohol; at 20 ℃; for 2h;

With formic acid; In dichloromethane; for 2h;

Reference yield:

: 95-68-1
2,4-Xylidine

: 1429347-23-8
N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium iodide; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] / water / 1 h / 170 °C / Microwave irradiation

2.1: pyridine / 0.5 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.77 h / -78 - -70 °C / Inert atmosphere

3.2: 1.02 h / -78 °C

4.1: hydrogenchloride / isopropyl alcohol / 2 h / 20 °C

4.2: 2 h

With pyridine; hydrogenchloride; n-butyllithium; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; potassium iodide; In tetrahydrofuran; hexane; water; isopropyl alcohol;

Reference yield:

: 95-66-9
2,4-dimethylchlorobenzene

: 1429347-23-8
N-(2,4-dimethylphenyl)-4-(2-hydroxy-1-(2H-tetrazol-5-yl)propan-2-yl)-N-isobutylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: {1,3-bis[2,6-bis(1-methylethyl)phenyl]-2-imidazolidinyl}(chloro)(2-methyl-2-propen-1-yl)palladium; lithium hexamethyldisilazane / tetrahydrofuran / 0.75 h / 70 °C / Inert atmosphere; Sealed tube

2.1: pyridine / 0.5 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.77 h / -78 - -70 °C / Inert atmosphere

3.2: 1.02 h / -78 °C

4.1: hydrogenchloride / isopropyl alcohol / 2 h / 20 °C

4.2: 2 h

With pyridine; hydrogenchloride; n-butyllithium; {1,3-bis[2,6-bis(1-methylethyl)phenyl]-2-imidazolidinyl}(chloro)(2-methyl-2-propen-1-yl)palladium; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; isopropyl alcohol;