O,O'-di-n-propyl isothiocyanato(phenyl)methylphosphonate

Base Information

Chemical Name:O,O'-di-n-propyl isothiocyanato(phenyl)methylphosphonate
CAS No.:1192761-58-2
Molecular Formula:C₁₄H₂₀NO₃PS
Molecular Weight:313.357
Hs Code.:

Synonyms:O,O'-di-n-propyl isothiocyanato(phenyl)methylphosphonate

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Chemical Property of O,O'-di-n-propyl isothiocyanato(phenyl)methylphosphonate

Chemical Property:

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Technology Process of O,O'-di-n-propyl isothiocyanato(phenyl)methylphosphonate

There total 7 articles about O,O'-di-n-propyl isothiocyanato(phenyl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 75-15-0,12122-00-8
carbon disulfide

: di-n-propyl amino(phenyl)methylphosphonate

: 1192761-58-2
O,O'-di-n-propyl isothiocyanato(phenyl)methylphosphonate

Guidance literature:: carbon disulfide; di-n-propyl amino(phenyl)methylphosphonate; With triethylamine; In diethyl ether; at 0 - 23 ℃; for 3h;

With bis(trichloromethyl) carbonate; In diethyl ether; at 23 ℃; for 3h;
DOI:10.3390/molecules15085112

Reference yield:

: 100-52-7
benzaldehyde

: 1192761-58-2
O,O'-di-n-propyl isothiocyanato(phenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium hydroxide / water / 5 h / Inert atmosphere; Reflux

2.1: 70 °C / Inert atmosphere; Neat (no solvent)

3.1: toluene-4-sulfonic acid / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3.2: 0.5 h / 20 °C / Inert atmosphere

4.1: Inert atmosphere

4.2: 4 h / 0 - 25 °C / Inert atmosphere

4.3: 2 h / 25 °C / Inert atmosphere

With ammonium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; water;
DOI:10.1007/s11426-010-4179-5

Reference yield:

: 92-29-5
hydrobenzamide

: 1192761-58-2
O,O'-di-n-propyl isothiocyanato(phenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 70 °C / Inert atmosphere; Neat (no solvent)

2.1: toluene-4-sulfonic acid / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

3.1: Inert atmosphere

3.2: 4 h / 0 - 25 °C / Inert atmosphere

3.3: 2 h / 25 °C / Inert atmosphere

With toluene-4-sulfonic acid; In tetrahydrofuran;
DOI:10.1007/s11426-010-4179-5