[(S)-7-(4-Methoxybenzyloxy)hept-1-en-4-yloxy](tert-butyl)dimethylsilane

Base Information

Chemical Name:[(S)-7-(4-Methoxybenzyloxy)hept-1-en-4-yloxy](tert-butyl)dimethylsilane
CAS No.:1292297-92-7
Molecular Formula:C₂₁H₃₆O₃Si
Molecular Weight:364.601
Hs Code.:

Synonyms:[(S)-7-(4-Methoxybenzyloxy)hept-1-en-4-yloxy](tert-butyl)dimethylsilane

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Chemical Property of [(S)-7-(4-Methoxybenzyloxy)hept-1-en-4-yloxy](tert-butyl)dimethylsilane

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Technology Process of [(S)-7-(4-Methoxybenzyloxy)hept-1-en-4-yloxy](tert-butyl)dimethylsilane

There total 14 articles about [(S)-7-(4-Methoxybenzyloxy)hept-1-en-4-yloxy](tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1292297-91-6
(S)-7-(4-methoxybenzyloxy)hept-1-en-4-ol

: 69739-34-0
t-butyldimethylsiyl triflate

: 1292297-92-7
[(S)-7-(4-Methoxybenzyloxy)hept-1-en-4-yloxy](tert-butyl)dimethylsilane

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1055/s-0030-1258389

Reference yield: 88.0%

: 1292297-91-6
(S)-7-(4-methoxybenzyloxy)hept-1-en-4-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1292297-92-7
[(S)-7-(4-Methoxybenzyloxy)hept-1-en-4-yloxy](tert-butyl)dimethylsilane

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃;
DOI:10.1246/bcsj.20100197

Reference yield:

: 119649-45-5
4-(p-methoxybenzyloxy)butan-1-ol

: 1292297-92-7
[(S)-7-(4-Methoxybenzyloxy)hept-1-en-4-yloxy](tert-butyl)dimethylsilane

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / -78 °C

1.2: -78 °C

2.1: tetrahydrofuran / 1 h / 0 °C

2.2: 0 °C

3.1: chlorodicarbonyl(1-(isopropylamino)-2,3,4,5-tetraphenylcyclopentadienyl) ruthenium (II); Candida antartica lipase B immobilized on acrylic resin; potassium tert-butylate; sodium carbonate / toluene / 20 °C / Inert atmosphere; Enzymatic reaction

4.1: methanol; potassium carbonate

5.1: 1H-imidazole / dichloromethane / 20 °C

With 1H-imidazole; methanol; chlorodicarbonyl(1-(isopropylamino)-2,3,4,5-tetraphenylcyclopentadienyl) ruthenium (II); oxalyl dichloride; Candida antartica lipase B immobilized on acrylic resin; potassium tert-butylate; sodium carbonate; potassium carbonate; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; toluene; 1.1: Swern oxidation / 1.2: Swern oxidation;
DOI:10.1246/bcsj.20100197