3-(4-hydroxy-3,5-dimethoxyphenyl)-3-(2-hydroxy-5-(2-hydroxyethyl)phenyl)propanoic acid

Base Information

Chemical Name:3-(4-hydroxy-3,5-dimethoxyphenyl)-3-(2-hydroxy-5-(2-hydroxyethyl)phenyl)propanoic acid
CAS No.:1552302-05-2
Molecular Formula:C₁₉H₂₂O₇
Molecular Weight:362.379
Hs Code.:

Synonyms:3-(4-hydroxy-3,5-dimethoxyphenyl)-3-(2-hydroxy-5-(2-hydroxyethyl)phenyl)propanoic acid

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Chemical Property of 3-(4-hydroxy-3,5-dimethoxyphenyl)-3-(2-hydroxy-5-(2-hydroxyethyl)phenyl)propanoic acid

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Technology Process of 3-(4-hydroxy-3,5-dimethoxyphenyl)-3-(2-hydroxy-5-(2-hydroxyethyl)phenyl)propanoic acid

There total 5 articles about 3-(4-hydroxy-3,5-dimethoxyphenyl)-3-(2-hydroxy-5-(2-hydroxyethyl)phenyl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1552301-95-7
2-[4-(4-hydroxy-3,5-dimethoxyphenyl)-2-oxochroman-6-yl]ethyl methyl carbonate

: 1552302-05-2
3-(4-hydroxy-3,5-dimethoxyphenyl)-3-(2-hydroxy-5-(2-hydroxyethyl)phenyl)propanoic acid

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; at 25 ℃; for 24h;
DOI:10.1039/c3nj01180a

Reference yield:

: 90985-68-5,113158-15-9
(E)-4-acetoxy-3,5-dimethoxycinnamic acid

: 1552302-05-2
3-(4-hydroxy-3,5-dimethoxyphenyl)-3-(2-hydroxy-5-(2-hydroxyethyl)phenyl)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 8 h / 25 °C

2: trifluoroacetic acid / 5 h / Reflux

3: potassium hydroxide / tetrahydrofuran / 24 h / 25 °C

With potassium carbonate; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; acetone;
DOI:10.1039/c3nj01180a

Reference yield:

: 501-94-0
p-hydroxyphenethyl alcohol

: 1552302-05-2
3-(4-hydroxy-3,5-dimethoxyphenyl)-3-(2-hydroxy-5-(2-hydroxyethyl)phenyl)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 8 h / Reflux

2: trifluoroacetic acid / 5 h / Reflux

3: potassium hydroxide / tetrahydrofuran / 24 h / 25 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran;
DOI:10.1039/c3nj01180a