4-chloroselenobenzamide

Base Information

• Chemical Name: 4-chloroselenobenzamide
• CAS No.: 67213-28-9
• Molecular Formula: C₇H₆ClNSe
• Molecular Weight: 218.544
• Mol file: 67213-28-9.mol

Synonyms:4-chloroselenobenzamide

Chemical Property of 4-chloroselenobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-chloroselenobenzamide

There total 4 articles about 4-chloroselenobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-Cyanochlorobenzene (623-03-0) → 4-chloroselenobenzamide (67213-28-9)

Guidance literature:

With selenium; carbon monoxide; water; triethylamine; In tetrahydrofuran; at 100 ℃; for 5h; under 3800 Torr;

DOI:10.1021/jo00203a020

Reference yield: 86.0%

4-Cyanochlorobenzene (623-03-0) + potassium 4-methylbenzenecarboselenoate → 4-chloroselenobenzamide (67213-28-9)

Guidance literature:

With boron trifluoride diethyl etherate; In tetrahydrofuran; at 0 ℃; for 5h;

DOI:10.1246/cl.1998.1287

Reference yield: 15.0%

4-Cyanochlorobenzene (623-03-0) → 1,2-bis(4-cyanophenyl) diselenide (84019-98-7) + 4-chloroselenobenzamide (67213-28-9)

Guidance literature:

With sodium perchlorate; In N,N-dimethyl-formamide; for 20h; Yield given; electrolysis (Se=kat., Pt=anod.);

upstream raw materials:

4-Cyanochlorobenzene

Downstream raw materials:

5-(4-Chlorphenyl)-3,3-bis(trifluormethyl)-3H-1,2,4-diselenazol

2-(4-chlorophenyl)-4-phenylselenazole

5-(tert-Butylimino)-2-(4-chlorphenyl)-4,4-bis(trifluormethyl)-Δ²-1,3-selenazolin

2-(4-chloro-phenyl)-4-methyl-selenazole