(S)-((3S,4S)-7-(tert-butyldiphenylsilyloxy)-2,4-dimethylhept-1-en-3-yl) 4-(6-methoxy-5-(methoxymethoxy)-7-methylbenzofuran-2-yl)pentanoate

Base Information

Chemical Name:(S)-((3S,4S)-7-(tert-butyldiphenylsilyloxy)-2,4-dimethylhept-1-en-3-yl) 4-(6-methoxy-5-(methoxymethoxy)-7-methylbenzofuran-2-yl)pentanoate
CAS No.:1189524-45-5
Molecular Formula:C₄₂H₅₆O₇Si
Molecular Weight:700.988
Hs Code.:

Synonyms:(S)-((3S,4S)-7-(tert-butyldiphenylsilyloxy)-2,4-dimethylhept-1-en-3-yl) 4-(6-methoxy-5-(methoxymethoxy)-7-methylbenzofuran-2-yl)pentanoate

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Chemical Property of (S)-((3S,4S)-7-(tert-butyldiphenylsilyloxy)-2,4-dimethylhept-1-en-3-yl) 4-(6-methoxy-5-(methoxymethoxy)-7-methylbenzofuran-2-yl)pentanoate

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Technology Process of (S)-((3S,4S)-7-(tert-butyldiphenylsilyloxy)-2,4-dimethylhept-1-en-3-yl) 4-(6-methoxy-5-(methoxymethoxy)-7-methylbenzofuran-2-yl)pentanoate

There total 1 articles about (S)-((3S,4S)-7-(tert-butyldiphenylsilyloxy)-2,4-dimethylhept-1-en-3-yl) 4-(6-methoxy-5-(methoxymethoxy)-7-methylbenzofuran-2-yl)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1189524-38-6
(S)-4-(6-methoxy-5-(methoxymethoxy)-7-methylbenzofuran-2-yl)pentanoic acid

: 1189524-37-5
(3S,4S)-7-(tert-butyldiphenylsilyloxy)-2,4-dimethylhept-1-en-3-ol

: 1189524-45-5
(S)-((3S,4S)-7-(tert-butyldiphenylsilyloxy)-2,4-dimethylhept-1-en-3-yl) 4-(6-methoxy-5-(methoxymethoxy)-7-methylbenzofuran-2-yl)pentanoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.200900522

Reference yield:

: 1189524-45-5
(S)-((3S,4S)-7-(tert-butyldiphenylsilyloxy)-2,4-dimethylhept-1-en-3-yl) 4-(6-methoxy-5-(methoxymethoxy)-7-methylbenzofuran-2-yl)pentanoate

: 18162-48-6
tert-butyldimethylsilyl chloride

: C₄₈H₇₀O₇Si₂

Guidance literature:: (S)-((3S,4S)-7-(tert-butyldiphenylsilyloxy)-2,4-dimethylhept-1-en-3-yl) 4-(6-methoxy-5-(methoxymethoxy)-7-methylbenzofuran-2-yl)pentanoate; With lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 0.75h; Inert atmosphere;

tert-butyldimethylsilyl chloride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 - 20 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1002/anie.200900522