N-[1-(3-tert-Butyl-1-methyl-thioureido)-2-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-eth-(Z)-ylidene]-4-methyl-benzenesulfonamide

Base Information

• Chemical Name: N-[1-(3-tert-Butyl-1-methyl-thioureido)-2-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-eth-(Z)-ylidene]-4-methyl-benzenesulfonamide
• CAS No.: 83325-01-3
• Molecular Formula: C₃₉H₄₀N₃O₂PS₂
• Molecular Weight: 677.871

Synonyms:N-[1-(3-tert-Butyl-1-methyl-thioureido)-2-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-eth-(Z)-ylidene]-4-methyl-benzenesulfonamide

Chemical Property of N-[1-(3-tert-Butyl-1-methyl-thioureido)-2-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-eth-(Z)-ylidene]-4-methyl-benzenesulfonamide

Chemical Property:

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Technology Process of N-[1-(3-tert-Butyl-1-methyl-thioureido)-2-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-eth-(Z)-ylidene]-4-methyl-benzenesulfonamide

There total 3 articles about N-[1-(3-tert-Butyl-1-methyl-thioureido)-2-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-eth-(Z)-ylidene]-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

N-(4-tert-butylimino-3-methyl-[1,3]thiazetidin-2-ylidene)-toluene-4-sulfonamide (36791-67-0) + triphenyl(phenylmethylene)phosphorane (16721-45-2) → N-tert-butyl-N'-tosylbenzylamidine + N-[1-(3-tert-Butyl-1-methyl-thioureido)-2-phenyl-2-(triphenyl-λ5-phosphanylidene)-eth-(Z)-ylidene]-4-methyl-benzenesulfonamide (83325-01-3)

Guidance literature:

Ambient temperature;

DOI:10.1016/S0040-4039(00)88446-4

Reference yield: 8.0%

N-(4-tert-butylimino-3-methyl-[1,3]thiazetidin-2-ylidene)-toluene-4-sulfonamide (36791-67-0) + triphenyl(phenylmethylene)phosphorane (16721-45-2) → N-tert-butyl-N'-tosylbenzylamidine + N-[1-(3-tert-Butyl-1-methyl-thioureido)-2-phenyl-2-(triphenyl-λ5-phosphanylidene)-eth-(Z)-ylidene]-4-methyl-benzenesulfonamide (83325-01-3) + triphenylphosphine sulfide (3878-45-3)

Guidance literature:

Ambient temperature;

DOI:10.1016/S0040-4039(00)88446-4

Reference yield:

benzyltriphenylphosphonium bromide (1449-46-3) → N-[1-(3-tert-Butyl-1-methyl-thioureido)-2-phenyl-2-(triphenyl-λ5-phosphanylidene)-eth-(Z)-ylidene]-4-methyl-benzenesulfonamide (83325-01-3)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / dimethylsulfoxide

2: 11 percent / Ambient temperature

With sodium hydride; In dimethyl sulfoxide;

DOI:10.1016/S0040-4039(00)88446-4

upstream raw materials:

N-(4-tert-butylimino-3-methyl-[1,3]thiazetidin-2-ylidene)-toluene-4-sulfonamide

triphenyl(phenylmethylene)phosphorane

benzyltriphenylphosphonium bromide

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