methyl (phenyl 5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-α-D-galactonon-2-ulopyranoside)onate

Base Information

Chemical Name:methyl (phenyl 5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-α-D-galactonon-2-ulopyranoside)onate
CAS No.:934415-78-8
Molecular Formula:C₁₇H₂₁NO₈S
Molecular Weight:399.422
Hs Code.:

Synonyms:methyl (phenyl 5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-α-D-galactonon-2-ulopyranoside)onate

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Chemical Property of methyl (phenyl 5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-α-D-galactonon-2-ulopyranoside)onate

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Technology Process of methyl (phenyl 5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-α-D-galactonon-2-ulopyranoside)onate

There total 3 articles about methyl (phenyl 5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-α-D-galactonon-2-ulopyranoside)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 934415-84-6
5-amino-4-hydroxy-2-phenylsulfanyl-6-(1,2,3-trihydroxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester

: 7693-46-1
4-Nitrophenyl chloroformate

: 934415-78-8
methyl (phenyl 5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-α-D-galactonon-2-ulopyranoside)onate

Guidance literature:: With sodium hydrogencarbonate; In water; acetonitrile; for 3h;
DOI:10.1016/j.tetlet.2006.12.061

Reference yield: 72.0%

: 7693-46-1
4-Nitrophenyl chloroformate

: 118977-25-6,118977-26-7
methyl (phenyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-galacto-2-nonulopyranoside)onate

: 934415-78-8
methyl (phenyl 5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-α-D-galactonon-2-ulopyranoside)onate

Guidance literature:: methyl (phenyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-galacto-2-nonulopyranoside)onate; With methanesulfonic acid; In methanol; for 24h; Heating;

4-Nitrophenyl chloroformate; With sodium hydrogencarbonate; In water; acetonitrile; at 0 ℃; for 3h;
DOI:10.1021/jo062431r

Reference yield:

: 118977-25-6,118977-26-7
methyl (phenyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-galacto-2-nonulopyranoside)onate

: 934415-78-8
methyl (phenyl 5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-α-D-galactonon-2-ulopyranoside)onate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / MsOH / methanol / 65 °C

2: 80 percent / NaHCO₃ / acetonitrile; H₂O / 3 h

With methanesulfonic acid; sodium hydrogencarbonate; In methanol; water; acetonitrile;
DOI:10.1016/j.tetlet.2006.12.061