[2-amino-N-(4-β-D-2,3,4,6-tetra-O-acetylgalactopyranosyloxy-3-nitrophenyl)methoxycarbonyl-4-benzyloxy-5-methoxy-1,4-phenylene]carbonyl (2S)-pyrrolidine-2-carboxaldehyde diethyldithioacetal

Base Information

Chemical Name:[2-amino-N-(4-β-D-2,3,4,6-tetra-O-acetylgalactopyranosyloxy-3-nitrophenyl)methoxycarbonyl-4-benzyloxy-5-methoxy-1,4-phenylene]carbonyl (2S)-pyrrolidine-2-carboxaldehyde diethyldithioacetal
CAS No.:1041181-51-4
Molecular Formula:C₄₆H₅₅N₃O₁₇S₂
Molecular Weight:986.085
Hs Code.:

[2-amino-N-(4-β-D-2,3,4,6-tetra-O-acetylgalactopyranosyloxy-3-nitrophenyl)methoxycarbonyl-4-benzyloxy-5-methoxy-1,4-phenylene]carbonyl (2S)-pyrrolidine-2-carboxaldehyde diethyldithioacetal

Synonyms:[2-amino-N-(4-β-D-2,3,4,6-tetra-O-acetylgalactopyranosyloxy-3-nitrophenyl)methoxycarbonyl-4-benzyloxy-5-methoxy-1,4-phenylene]carbonyl (2S)-pyrrolidine-2-carboxaldehyde diethyldithioacetal

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Chemical Property of [2-amino-N-(4-β-D-2,3,4,6-tetra-O-acetylgalactopyranosyloxy-3-nitrophenyl)methoxycarbonyl-4-benzyloxy-5-methoxy-1,4-phenylene]carbonyl (2S)-pyrrolidine-2-carboxaldehyde diethyldithioacetal

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Technology Process of [2-amino-N-(4-β-D-2,3,4,6-tetra-O-acetylgalactopyranosyloxy-3-nitrophenyl)methoxycarbonyl-4-benzyloxy-5-methoxy-1,4-phenylene]carbonyl (2S)-pyrrolidine-2-carboxaldehyde diethyldithioacetal

There total 1 articles about [2-amino-N-(4-β-D-2,3,4,6-tetra-O-acetylgalactopyranosyloxy-3-nitrophenyl)methoxycarbonyl-4-benzyloxy-5-methoxy-1,4-phenylene]carbonyl (2S)-pyrrolidine-2-carboxaldehyde diethyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: 127810-78-0
(2S)-N-(2-amino-4-benzyloxy-5-methoxybenzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal

: 290298-12-3
(2R,3S,4S,5R,6S)-2-(acetoxymethyl)-6-(4-(hydroxymethyl)-2-nitrophenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 1041181-51-4
[2-amino-N-(4-β-D-2,3,4,6-tetra-O-acetylgalactopyranosyloxy-3-nitrophenyl)methoxycarbonyl-4-benzyloxy-5-methoxy-1,4-phenylene]carbonyl (2S)-pyrrolidine-2-carboxaldehyde diethyldithioacetal

Guidance literature:: bis(trichloromethyl) carbonate; (2S)-N-(2-amino-4-benzyloxy-5-methoxybenzoyl)pyrrolidine-2-carbaldehyde diethyl dithioacetal; With triethylamine; In dichloromethane; for 0.416667h;

(2R,3S,4S,5R,6S)-2-(acetoxymethyl)-6-(4-(hydroxymethyl)-2-nitrophenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate; dibutyltin dilaurate; In dichloromethane; for 6h;

Reference yield: 76.0%

: 1041181-51-4
[2-amino-N-(4-β-D-2,3,4,6-tetra-O-acetylgalactopyranosyloxy-3-nitrophenyl)methoxycarbonyl-4-benzyloxy-5-methoxy-1,4-phenylene]carbonyl (2S)-pyrrolidine-2-carboxaldehyde diethyldithioacetal

: 1041181-54-7
(11S)-10-(4-β-D-2,3,4,6-tetra-O-acetyl-galactopyranosyloxy-3-nitro-phenyl)methoxycarbonyl-11-hydroxy-7-methoxy-1,2,3,10,11,11a-hexahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one

Guidance literature:: With calcium carbonate; mercury dichloride; In water; acetonitrile; for 12h;

Reference yield:

: 1041181-51-4
[2-amino-N-(4-β-D-2,3,4,6-tetra-O-acetylgalactopyranosyloxy-3-nitrophenyl)methoxycarbonyl-4-benzyloxy-5-methoxy-1,4-phenylene]carbonyl (2S)-pyrrolidine-2-carboxaldehyde diethyldithioacetal

: 1104078-09-2
C₂₈H₂₇N₃O₉

Guidance literature:: Multi-step reaction with 3 steps

1: calcium carbonate; mercury dichloride / water; acetonitrile / 12 h

2: methanol / sodium methylate / 0.5 h / 0 °C

3: water / β-galactosidase / 1.25 h / 37 °C / pH 7.2 / Enzymatic reaction; Aqueous phosphate buffer

With methanol; water; calcium carbonate; mercury dichloride; β-galactosidase; sodium methylate; In water; acetonitrile;