hydridochloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)

Base Information

Chemical Name:hydridochloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)
CAS No.:102849-31-0
Molecular Formula:C₄₃H₃₈ClOOsP₃
Molecular Weight:889.348
Hs Code.:

Synonyms:hydridochloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)

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Chemical Property of hydridochloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)

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Technology Process of hydridochloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)

There total 1 articles about hydridochloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 16971-31-6,36007-23-5
hydridocarbonylchlorotris(triphenylphosphine)osmium(II)

: 638-21-1
phenylphosphane

: 102849-31-0
hydridochloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)

Guidance literature:: In benzene; byproducts: P(C6H5)3; inert atmosphere; addn. of PH2Ph in benzene to suspn. of Os-complex in benzene; refluxing at 80°C for 3 h;; cooling; removal of volatiles under vac.; dissolving in CH2Cl2 and recrystn. with EtOH; elem. anal.;

Reference yield: 91.0%

: 102849-31-0
hydridochloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)

: 75-05-8,26809-02-9
acetonitrile

: 102849-33-2
chloro(phenylphosphine)(acetonitrile)carbonylbis(triphenylphosphine)osmium(II) perchlorate

Guidance literature:: With perchloric acid; In dichloromethane; acetonitrile; byproducts: H2; inert atmosphere; addn. of HClO4 in CH3CN) to Os-complex in CH2Cl2; stirring for 2.5 h;; removal of solvent under vac.; dissolving in CH2Cl2 and recrystn. with 2-propanol; elem. anal.;

Reference yield: 84.0%

: 102849-31-0
hydridochloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)

: 102747-25-1,102849-36-5
dichloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)

Guidance literature:: With hydrogenchloride; In ethanol; benzene; byproducts: H2; addn. of HCl in EtOH to soln. of Os-complex in benzene; refluxing for 6h; cooling; removal of solvent; recrystn. (CH2Cl2/EtOH); cis/trans isomer mixt. obtained; elem. anal.;